(2-Bromo-3,4-dimethoxyphenyl)methanol

Base Information

Chemical Name:(2-Bromo-3,4-dimethoxyphenyl)methanol
CAS No.:72912-38-0
Molecular Formula:C9H11BrO3
Molecular Weight:247.089
Hs Code.:
DSSTox Substance ID:DTXSID60546994
Nikkaji Number:J875.444F
Wikidata:Q82424977
Mol file:72912-38-0.mol

Synonyms:72912-38-0;(2-bromo-3,4-dimethoxyphenyl)methanol;Benzenemethanol, 2-bromo-3,4-dimethoxy-;2-Bromoveratryl-d3Alcohol;2-Bromoveratryl Alcohol;SCHEMBL147850;DTXSID60546994;AKOS024113335;AS-0245;CS-0378422;EN300-1913565

Suppliers and Price of (2-Bromo-3,4-dimethoxyphenyl)methanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2-BromoveratrylAlcohol
50mg
$ 165.00

Medical Isotopes, Inc.
2-BromoveratrylAlcohol
50 mg
$ 650.00

American Custom Chemicals Corporation
2-BROMOVERATRYL ALCOHOL 95.00%
5MG
$ 502.67

Total 3 raw suppliers

Chemical Property of (2-Bromo-3,4-dimethoxyphenyl)methanol

Chemical Property:

Melting Point:76-79 °C
Boiling Point:320.6±37.0 °C(Predicted)
PKA:13.77±0.10(Predicted)
PSA：38.69000
Density:1.475±0.06 g/cm3(Predicted)
LogP:1.95860
Storage Temp.:Refrigerator
Solubility.:Chloroform, Dichloromethane, Methanol
XLogP3:1.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:245.98916
Heavy Atom Count:13
Complexity:154

Purity/Quality:

99% ^*data from raw suppliers

2-BromoveratrylAlcohol ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C(=C(C=C1)CO)Br)OC
Uses 2-BroMoveratryl Alcohol can be used in the preparation of isoquinoline and dibenzoquinolizine derivatives as antibacterial agents.

Technology Process of (2-Bromo-3,4-dimethoxyphenyl)methanol

There total 10 articles about (2-Bromo-3,4-dimethoxyphenyl)methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 55171-60-3
2-bromo-3,4-dimethoxybenzylaldehyde

: 72912-38-0
(2-bromo-3,4-dimethoxyphenyl)methanol

Guidance literature:: With sodium tetrahydroborate; In tetrahydrofuran; methanol; for 2h;
DOI:10.1021/jo982451w

Reference yield:

: 621-59-0
isovanillin

: 72912-38-0
(2-bromo-3,4-dimethoxyphenyl)methanol

Guidance literature:: Multi-step reaction with 3 steps

1: 36 percent / Br₂

2: 80 percent / K₂CO₃ / dimethylformamide / 0.08 h / Heating

3: NaBH₄ / aq. ethanol / 1 h / 25 °C

With sodium tetrahydroborate; bromine; potassium carbonate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00161a029

Reference yield:

: 2973-58-2
2-bromoisovanillin

: 72912-38-0
(2-bromo-3,4-dimethoxyphenyl)methanol

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / K₂CO₃ / dimethylformamide / 0.08 h / Heating

2: NaBH₄ / aq. ethanol / 1 h / 25 °C

With sodium tetrahydroborate; potassium carbonate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00161a029