19,24-Dioctadecyldotetracontane

Base Information

Chemical Name:19,24-Dioctadecyldotetracontane
CAS No.:72942-95-1
Molecular Formula:C₇₈H₁₅₈
Molecular Weight:1096.11
Hs Code.:
DSSTox Substance ID:DTXSID30502067
Nikkaji Number:J275.459B
Wikidata:Q82354843

Synonyms:19,24-DIOCTADECYLDOTETRACONTANE;72942-95-1;DTXSID30502067

Suppliers and Price of 19,24-Dioctadecyldotetracontane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 19,24-Dioctadecyldotetracontane

Chemical Property:

Vapor Pressure:0mmHg at 25°C
XLogP3:41.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:73
Exact Mass:1095.23635504
Heavy Atom Count:78
Complexity:831

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCCCCCCCCCCCCCCCC(CCCCCCCCCCCCCCCCCC)CCCCC(CCCCCCCCCCCCCCCCCC)CCCCCCCCCCCCCCCCCC

Technology Process of 19,24-Dioctadecyldotetracontane

There total 11 articles about 19,24-Dioctadecyldotetracontane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 19,24-dioctadecyl-19-dotetracontene

: 72942-95-1
19,24-dioctadecyldotetracontane

Guidance literature:: With hydrogen; palladium on activated charcoal; In cyclohexane; at 40 ℃; for 20h; under 7500.6 Torr;
DOI:10.1055/s-1993-25968

Reference yield:

: 112-89-0
1-Bromooctadecane

: 72942-95-1
19,24-dioctadecyldotetracontane

Guidance literature:: Multi-step reaction with 7 steps

1: 73 percent / 1.) Mg, 1,2-dibromoethane / tetrahydrofuran / 1.) reflux, 3.5 h; 2.) reflux, 5 h

2: 1.) p-TsOH*H₂O; 2.) hydrogen / 2.) 10percent Pd-C / 1.) benzene, reflux, 2 h; 2.) cyclohexane, 40 deg C, 15 bar, 18 h

3: 74 percent / PCC / CH₂Cl₂ / 16 h / Ambient temperature

4: 67 percent / BuLi / tetrahydrofuran; hexane / 0.5 h / Ambient temperature

5: 70 percent / hydrogen / 10percent Pd-C / cyclohexane / 20 h / 40 °C / 9000.7 Torr

6: p-TsOH*H₂O / benzene / 2 h / Heating

7: 84 percent / hydrogen / 10percent Pd-C / cyclohexane / 20 h / 40 °C / 7500.6 Torr

With n-butyllithium; hydrogen; toluene-4-sulfonic acid; magnesium; ethylene dibromide; pyridinium chlorochromate; palladium on activated charcoal; In tetrahydrofuran; hexane; dichloromethane; cyclohexane; benzene;
DOI:10.1055/s-1993-25968

Reference yield:

: 6654-36-0
methyl 6-oxohexanoate

: 72942-95-1
19,24-dioctadecyldotetracontane

Guidance literature:: Multi-step reaction with 7 steps

1: 73 percent / 1.) Mg, 1,2-dibromoethane / tetrahydrofuran / 1.) reflux, 3.5 h; 2.) reflux, 5 h

2: 1.) p-TsOH*H₂O; 2.) hydrogen / 2.) 10percent Pd-C / 1.) benzene, reflux, 2 h; 2.) cyclohexane, 40 deg C, 15 bar, 18 h

3: 74 percent / PCC / CH₂Cl₂ / 16 h / Ambient temperature

4: 67 percent / BuLi / tetrahydrofuran; hexane / 0.5 h / Ambient temperature

5: 70 percent / hydrogen / 10percent Pd-C / cyclohexane / 20 h / 40 °C / 9000.7 Torr

6: p-TsOH*H₂O / benzene / 2 h / Heating

7: 84 percent / hydrogen / 10percent Pd-C / cyclohexane / 20 h / 40 °C / 7500.6 Torr

With n-butyllithium; hydrogen; toluene-4-sulfonic acid; magnesium; ethylene dibromide; pyridinium chlorochromate; palladium on activated charcoal; In tetrahydrofuran; hexane; dichloromethane; cyclohexane; benzene;
DOI:10.1055/s-1993-25968