6-Methyl-2-[(trimethylsilyl)methyl]cyclohex-3-ene-1-carbaldehyde

Base Information

Chemical Name:6-Methyl-2-[(trimethylsilyl)methyl]cyclohex-3-ene-1-carbaldehyde
CAS No.:72952-63-7
Molecular Formula:C12H22OSi
Molecular Weight:210.392
Hs Code.:
DSSTox Substance ID:DTXSID30503135

Synonyms:72952-63-7;DTXSID30503135;6-Methyl-2-[(trimethylsilyl)methyl]cyclohex-3-ene-1-carbaldehyde

Suppliers and Price of 6-Methyl-2-[(trimethylsilyl)methyl]cyclohex-3-ene-1-carbaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-Methyl-2-[(trimethylsilyl)methyl]cyclohex-3-ene-1-carbaldehyde

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:210.143991855
Heavy Atom Count:14
Complexity:227

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1CC=CC(C1C=O)C[Si](C)(C)C

Technology Process of 6-Methyl-2-[(trimethylsilyl)methyl]cyclohex-3-ene-1-carbaldehyde

There total 3 articles about 6-Methyl-2-[(trimethylsilyl)methyl]cyclohex-3-ene-1-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 72952-73-9
(E)-2,4-pentadienyltrimethylsilane

: 123-73-9,4170-30-3
crotonaldehyde

: 72952-63-7
6-Methyl-2-trimethylsilanylmethyl-cyclohex-3-enecarbaldehyde

Guidance literature:: titanium tetrachloride; In dichloromethane; at -40 - 5 ℃; for 0.0833333h;
DOI:10.1021/jo01297a053

Reference yield: 40.0%

: 123-73-9,4170-30-3
trans-Crotonaldehyde

: 72952-73-9
(E)-2,4-pentadienyltrimethylsilane

: 72952-63-7
6-Methyl-2-trimethylsilanylmethyl-cyclohex-3-enecarbaldehyde

Guidance literature:: With boron trifluoride diethyl etherate; at -78 ℃; for 0.5h;
DOI:10.1246/cl.1983.1683

Reference yield:

: 54962-98-0
pentadienyl lithium

: 72952-63-7
6-Methyl-2-trimethylsilanylmethyl-cyclohex-3-enecarbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / tetrahydrofuran / Ambient temperature

2: 40 percent / TiCl₄ / CH₂Cl₂ / 0.08 h / -40 - 5 °C

titanium tetrachloride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo01297a053