4-[(E)-(4-Methylphenyl)diazenyl]-3,5-diphenyl-1,2-oxazole

Base Information

Chemical Name:4-[(E)-(4-Methylphenyl)diazenyl]-3,5-diphenyl-1,2-oxazole
CAS No.:72990-87-5
Molecular Formula:C₂₂H₁₇N₃O
Molecular Weight:339.396
Hs Code.:
DSSTox Substance ID:DTXSID10524520

Synonyms:72990-87-5;DTXSID10524520;4-[(E)-(4-Methylphenyl)diazenyl]-3,5-diphenyl-1,2-oxazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-[(E)-(4-Methylphenyl)diazenyl]-3,5-diphenyl-1,2-oxazole

Chemical Property:

XLogP3:5.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:339.137162174
Heavy Atom Count:26
Complexity:448

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC=C(C=C1)N=NC2=C(ON=C2C3=CC=CC=C3)C4=CC=CC=C4

Technology Process of 4-[(E)-(4-Methylphenyl)diazenyl]-3,5-diphenyl-1,2-oxazole

There total 6 articles about 4-[(E)-(4-Methylphenyl)diazenyl]-3,5-diphenyl-1,2-oxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 91816-24-9
3-Phenyl-4-(p-tolyl-hydrazono)-4H-isoxazole-5-thione

: phenylmagnesium bromide

: 72990-87-5
3,5-diphenyl-4-p-tolylazo-isoxazole

Guidance literature:: In diethyl ether; for 0.25h; Ambient temperature;

Reference yield: 15.0%

: 57573-52-1
4-methylbenzene diazonium

: 62260-73-5
3,5-Diphenyl-4-nitroisoxazoline

: 72990-87-5
3,5-diphenyl-4-p-tolylazo-isoxazole

Guidance literature:: With sodium hydroxide; In methanol; at 0 ℃; for 0.5h;

Reference yield:

: 91816-25-0
4-[2-(4-methylphenyl)hydrazinylidene]-3-phenyl-1,2-oxazol-5(4H)-one

: 72990-87-5
3,5-diphenyl-4-p-tolylazo-isoxazole

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / P₄S₁₀ / dioxane / 2 h / Heating

2: 55 percent / diethyl ether / 0.25 h / Ambient temperature

With tetraphosphorus decasulfide; In 1,4-dioxane; diethyl ether;