(E)-N'-(2-Chlorobenzylidene)-4-nitrobenzenesulfonohydrazide

Base Information

Chemical Name:(E)-N'-(2-Chlorobenzylidene)-4-nitrobenzenesulfonohydrazide
CAS No.:6975-51-5
Molecular Formula:C13H10 Cl N3 O4 S
Molecular Weight:339.759
Hs Code.:
NSC Number:22618
Mol file:6975-51-5.mol

Synonyms:NSC22618;(E)-N'-(2-Chlorobenzylidene)-4-nitrobenzenesulfonohydrazide;NSC-22618;6975-51-5

Suppliers and Price of (E)-N'-(2-Chlorobenzylidene)-4-nitrobenzenesulfonohydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of (E)-N'-(2-Chlorobenzylidene)-4-nitrobenzenesulfonohydrazide

Chemical Property:

Boiling Point:525.631oC at 760 mmHg
Flash Point:271.692oC
PSA：112.73000
Density:1.482g/cm3
LogP:4.55550
XLogP3:3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:4
Exact Mass:339.0080547
Heavy Atom Count:22
Complexity:506

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C(=C1)C=NNS(=O)(=O)C2=CC=C(C=C2)[N+](=O)[O-])Cl
Isomeric SMILES:C1=CC=C(C(=C1)/C=N/NS(=O)(=O)C2=CC=C(C=C2)[N+](=O)[O-])Cl

Technology Process of (E)-N'-(2-Chlorobenzylidene)-4-nitrobenzenesulfonohydrazide

There total 2 articles about (E)-N'-(2-Chlorobenzylidene)-4-nitrobenzenesulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 2937-05-5
4-nitrobenzenesulfonohydrazide

: 89-98-5
2-chloro-benzaldehyde

: 6975-51-5
(E)-N'-(2-chlorobenzylidene)-4-nitrobenzenesulfonohydrazide

Guidance literature:: In ethanol; Heating;
DOI:10.1016/j.tet.2019.130534

Reference yield:

: 6975-51-5
(E)-N'-(2-chlorobenzylidene)-4-nitrobenzenesulfonohydrazide

Guidance literature:: /BRN= 3404107/;
DOI:10.1021/jo01093a010

Reference yield: 62.8%

: 1005500-77-5
N,4-dimethyl-N-(phenylethynyl)benzenesulfonamide

: 6975-51-5
(E)-N'-(2-chlorobenzylidene)-4-nitrobenzenesulfonohydrazide

: N-((E)-1-(2-((E)-2-chlorobenzylidene)-1-((4-nitrophenyl)sulfonyl)hydrazinyl)-2-phenylvinyl)-N,4-dimethylbenzenesulfonamide

Guidance literature:: With silver trifluoromethanesulfonate; potassium carbonate; In 1,2-dichloro-ethane; at 40 ℃; for 4h; stereoselective reaction; Schlenk technique; Sealed tube; Inert atmosphere; Heating;
DOI:10.1016/j.tet.2019.130534