Oxybis(diethylborane)

Base Information

Chemical Name:Oxybis(diethylborane)
CAS No.:7318-84-5
Molecular Formula:C8H20B2O
Molecular Weight:153.868
Hs Code.:
Mol file:7318-84-5.mol

Synonyms:Bis-diaethylboryl-aether;Diaethylborinsaeure-anhydrid;DIETHYLBORINIC ANHYDRIDE;Diaethylborsaeure-anhydrid;tetraethyldiboroxane;Tetraaethyl-diboroxan;tetraethyl-diboroxane;

Suppliers and Price of Oxybis(diethylborane)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of Oxybis(diethylborane)

Chemical Property:

Vapor Pressure:2.09mmHg at 25°C
PSA：9.23000
LogP:3.06560

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Oxybis(diethylborane)

There total 12 articles about Oxybis(diethylborane) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 159087-72-6
rac-9-{(dimethylamino)ethylboryloxy}-10-ethyl-10-(1-ethylethenyl)-9-borabicyclo{3.3.2}decane

: 5518-25-2
Diethylborane

: 2,3-(1,5-cyclooctandiyl)-3,4,6-triethyl-1,2,6-oxadiborinane

: 97-94-9
triethyl borane

: 7397-47-9
(dimethylamino)diethylborane

: 7318-84-5
Tetraethyldiboroxan

: 3043-60-5
triethylboroxine

Guidance literature:: With ethene; In neat (no solvent); byproducts: H2; under Ar, combined at -78°C, warmed to room temp., warmed to 95°C, heated for 2 h at 110-120°C, ethene passed at 40°C; removal of volatile compds. in vac., distn. in vac.;

Reference yield: 18.0%

: 138517-94-9
potassium 2,2,3,4,5-pentaethyl-2,5-dihydro-1,2,5-oxadiboratolate

: 593-81-7
trimethylamine hydrochloride

: 139688-17-8
diethyl(cis-1-ethyl-1-butenyl)borane

: 139688-18-9
2,3,3,4,5-pentaethyl-1,2,5-oxadiborolane

: 139688-19-0
1,3-diethyl-1,3-bis(cis-1-ethyl-1-butenyl)-1,3,2-diboroxane

: 87826-03-7
((C₂H₅)BO)3*(CH₃)3N

: 7318-84-5
Tetraethyldiboroxan

Guidance literature:: In tetrahydrofuran; byproducts: trimethyl amine, KCl; Ar atmosphere; refluxing (42 h); further products; filtration of KCl, partial evapn. (14 Torr), distn. (20-52°C, 0.001 Torr); elem. anal.;

Reference yield: 8.0%

: 138517-94-9
potassium 2,2,3,4,5-pentaethyl-2,5-dihydro-1,2,5-oxadiboratolate

: 139688-17-8
diethyl(cis-1-ethyl-1-butenyl)borane

: 139688-18-9
2,3,3,4,5-pentaethyl-1,2,5-oxadiborolane

: 1739-53-3
ethyl-dichloro-borane

: 7318-84-5
Tetraethyldiboroxan

: 3043-60-5
triethylboroxine

Guidance literature:: With hydrogenchloride; In diethyl ether; byproducts: trimethyl amine, KCl; Ar atmosphere; stirring (room temp., 2 h); not isolated or sepd.; (11)B-NMR spectroscopy;