11-(Diphenylphosphoryl)undecanoic acid

Base Information

Chemical Name:11-(Diphenylphosphoryl)undecanoic acid
CAS No.:73367-78-9
Molecular Formula:C23H31O3P
Molecular Weight:386.471
Hs Code.:
DSSTox Substance ID:DTXSID40396595
Nikkaji Number:J1.324.531B
Wikidata:Q82197385
ChEMBL ID:CHEMBL1566788

Synonyms:11-(diphenylphosphoryl)undecanoic acid;73367-78-9;MLS000777771;CHEMBL1566788;SCHEMBL10780224;DTXSID40396595;HMS2760H15;STK532950;AKOS005465052;11-(Diphenylphosphinyl)undecanoic acid;SMR000414101;11-(Diphenyl-phosphinoyl)-undecanoic acid

Suppliers and Price of 11-(Diphenylphosphoryl)undecanoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 11-(Diphenylphosphoryl)undecanoic acid

Chemical Property:

XLogP3:5.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:13
Exact Mass:386.20108184
Heavy Atom Count:27
Complexity:429

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)P(=O)(CCCCCCCCCCC(=O)O)C2=CC=CC=C2

Technology Process of 11-(Diphenylphosphoryl)undecanoic acid

There total 4 articles about 11-(Diphenylphosphoryl)undecanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 2834-05-1
11-bromoundecanoic acid

: 4559-70-0
Diphenylphosphine oxide

: 73367-78-9
11-diphenylphosphinoylundecanoic acid

Guidance literature:

Reference yield: 75.0%

: 7530-96-3
(11-carboxyundecyl)triphenylphosphonium bromide

: 73367-78-9
11-diphenylphosphinoylundecanoic acid

Guidance literature:: With sodium hydride; 1.) DMSO, 0 deg C, 5 min, 2.) THF, room temp., 36 h, 3.) 9-anthraldehyde, room temp., 6 d, 4.) aq. HCl;
DOI:10.1021/jo01299a040

Reference yield:

: 60633-18-3
(3-carboxy-propyl)triphenylphosphonium chloride

: 73367-78-9
11-diphenylphosphinoylundecanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 19 percent / NaH / 1.) DMSO, 0 deg C, 10 min, 2.) THF, room temp., 4 d, 3.) aq. HCl

2: 75 percent / toluene / 30 h / Heating

3: 58 percent / NaOC₂H₅ / dimethylformamide / 24 h / Ambient temperature

With sodium ethanolate; sodium hydride; In N,N-dimethyl-formamide; toluene;
DOI:10.1021/jo01299a040