[2,4'-Bipyridine]-3,3'-dicarboxylic acid

Base Information

• Chemical Name: [2,4'-Bipyridine]-3,3'-dicarboxylic acid
• CAS No.: 4433-02-7
• Molecular Formula: C12H8N2O4
• Molecular Weight: 244.207
• Hs Code.: 2933399090
• Mol file: 4433-02-7.mol

Synonyms:[2,4']Bipyridyl-3,3'-dicarbonsaeure;[2,4'-Bipyridine]-3,3'-dicarboxylic acid;

Chemical Property of [2,4'-Bipyridine]-3,3'-dicarboxylic acid

Chemical Property:

• Melting Point: 275 °C
• Boiling Point: 450.3±40.0 °C(Predicted)
• PSA: 100.38000
• Density: 1.469±0.06 g/cm3(Predicted)
• LogP: 1.54000

Purity/Quality:

95% ^*data from raw suppliers

[2,4'-Bipyridine]-3,3'-dicarboxylicacid 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of [2,4'-Bipyridine]-3,3'-dicarboxylic acid

There total 1 articles about [2,4'-Bipyridine]-3,3'-dicarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,8-phenanthroline (230-30-8) → [2,4']bipyridyl-3,3'-dicarboxylic acid (4433-02-7)

Guidance literature:

With sodium hydroxide; potassium permanganate;

DOI:10.1039/jr9580001574

Reference yield:

[2,4']bipyridyl-3,3'-dicarboxylic acid (4433-02-7) → 4-(2-pyridyl)pyridine (581-47-5)

Guidance literature:

With copper; nitrobenzene; at 205 - 210 ℃;

DOI:10.1039/jr9580001574

Reference yield:

[2,4']bipyridyl-3,3'-dicarboxylic acid (4433-02-7) → iodure de 1-methyl-4-(2-pyridyl)pyridinium (110462-45-8)

Guidance literature:

Multi-step reaction with 2 steps

1: copper-powder; nitrobenzene / 205 - 210 °C

2: ethanol / 100 - 110 °C

With ethanol; copper; nitrobenzene;

DOI:10.1039/jr9580001574

upstream raw materials:

1,8-phenanthroline

Downstream raw materials:

4-(2-pyridyl)pyridine

iodure de 1-methyl-4-(2-pyridyl)pyridinium