4-bromo-N-[(E)-(dimethylamino)methylidene]benzamide

Base Information

Chemical Name:4-bromo-N-[(E)-(dimethylamino)methylidene]benzamide
CAS No.:73823-15-1
Molecular Formula:C10H11BrN2O
Molecular Weight:255.114
Hs Code.:
DSSTox Substance ID:DTXSID30502224

Synonyms:4-bromo-N-[(E)-(dimethylamino)methylidene]benzamide;73823-15-1;SCHEMBL1438906;SCHEMBL1438908;SCHEMBL11290394;DTXSID30502224;DXJSSPFNZHQYBX-KPKJPENVSA-N;DXJSSPFNZHQYBX-UHFFFAOYSA-N;4-bromo-N-((dimethylamino)methylene)benzamide;(E)-4-bromo-N-((dimethylamino)methylene)benzamide;(E)-4-bromo-N-(dimethylamino-methylene)-benzamide

Suppliers and Price of 4-bromo-N-[(E)-(dimethylamino)methylidene]benzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-bromo-N-[(E)-(dimethylamino)methylidene]benzamide

Chemical Property:

XLogP3:2.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:254.00548
Heavy Atom Count:14
Complexity:220

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(C)C=NC(=O)C1=CC=C(C=C1)Br

Technology Process of 4-bromo-N-[(E)-(dimethylamino)methylidene]benzamide

There total 3 articles about 4-bromo-N-[(E)-(dimethylamino)methylidene]benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 698-67-9
p-bromobenzamide

: 4637-24-5
N,N-dimethyl-formamide dimethyl acetal

: 73823-15-1
4-bromo-N-((dimethylamino)methylene)benzamide

Guidance literature:: at 120 ℃; for 1.5h;
DOI:10.1055/s-1984-31030 DOI:10.1055/s-1980-28939

Reference yield:

: 586-76-5
4-Bromobenzoic acid

: 73823-15-1
4-bromo-N-((dimethylamino)methylene)benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / 2 h / Reflux

2: ammonium hydroxide / dichloromethane / 1 h / 0 - 20 °C

3: 2 h / 80 °C

With ammonium hydroxide; thionyl chloride; In dichloromethane;

Reference yield:

: 586-75-4
4-chlorobenzoyl chloride

: 73823-15-1
4-bromo-N-((dimethylamino)methylene)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium hydroxide / dichloromethane / 1 h / 0 - 20 °C

2: 2 h / 80 °C

With ammonium hydroxide; In dichloromethane;