[1,1'-Biphenyl]-2-carboxamide, 2'-methoxy-

Base Information

• Chemical Name: [1,1'-Biphenyl]-2-carboxamide, 2'-methoxy-
• CAS No.: 67856-55-7
• Molecular Formula: C14H13NO2
• Molecular Weight: 227.263
• European Community (EC) Number: 267-387-8
• UNII: 7FL86J2V23
• DSSTox Substance ID: DTXSID7070713
• Nikkaji Number: J287.527F
• Wikidata: Q81998108
• Mol file: 67856-55-7.mol

Synonyms:67856-55-7;2'-Methoxy-biphenyl-2-carboxylic acid amide;2-(2-methoxyphenyl)benzamide;[1,1'-Biphenyl]-2-carboxamide, 2'-methoxy-;2'-Methoxy-[1,1'-biphenyl]-2-carboxamide;EINECS 267-387-8;2'-methoxy[1,1'-biphenyl]-2-carboxamide;(1,1'-Biphenyl)-2-carboxamide, 2'-methoxy-;7FL86J2V23;2'-Methoxy(1,1'-biphenyl)-2-carboxamide;SCHEMBL527995;UNII-7FL86J2V23;DTXSID7070713;MFCD23713134;AB92586;2'-Methoxy-1,1'-biphenyl-2-carboxamide;2-Methoxy-biphenyl-2-carboxylic acid amide;CS-0196109;E92718

Chemical Property of [1,1'-Biphenyl]-2-carboxamide, 2'-methoxy-

Chemical Property:

• Boiling Point: 376.3°Cat760mmHg
• Flash Point: 175.3°C
• PSA: 53.31000
• Density: 1.151g/cm³
• LogP: 3.34530
• XLogP3: 1.9
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 3
• Exact Mass: 227.094628657
• Heavy Atom Count: 17
• Complexity: 267

Purity/Quality:

99% ^*data from raw suppliers

2'-Methoxy-biphenyl-2-carboxylic acid amide 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=CC=CC=C1C2=CC=CC=C2C(=O)N

Technology Process of [1,1'-Biphenyl]-2-carboxamide, 2'-methoxy-

There total 3 articles about [1,1'-Biphenyl]-2-carboxamide, 2'-methoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-lithio-4-methylanisole (70548-78-6) → 2'-methoxy(1,1'-biphenyl)-2-carboxamide (67856-55-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 59 percent / tetrahydrofuran

2: 1) singlet oxygen, 2.) LiOH / 2.) heating

With lithium hydroxide; oxygen; In tetrahydrofuran;

DOI:10.1246/cl.1987.19

Reference yield:

2-(2-Fluoro-phenyl)-4,5-dimethyl-oxazole (111603-46-4) → 2'-methoxy(1,1'-biphenyl)-2-carboxamide (67856-55-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 59 percent / tetrahydrofuran

2: 1) singlet oxygen, 2.) LiOH / 2.) heating

With lithium hydroxide; oxygen; In tetrahydrofuran;

DOI:10.1246/cl.1987.19

Reference yield:

2-(2'-Methoxy-biphenyl-2-yl)-4,5-dimethyl-oxazole (111603-47-5) → 2'-methoxybiphenyl-2-carboxylic acid (17296-28-5) + 2'-methoxy(1,1'-biphenyl)-2-carboxamide (67856-55-7)

Guidance literature:

With lithium hydroxide; oxygen; Yield given. Multistep reaction. Yields of byproduct given; 2.) heating;

DOI:10.1246/cl.1987.19

upstream raw materials:

2-(2'-Methoxy-biphenyl-2-yl)-4,5-dimethyl-oxazole

2-lithio-4-methylanisole

2-(2-Fluoro-phenyl)-4,5-dimethyl-oxazole

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