4-(4-CHLOROPHENYL)-1-(4-PYRIDYLCARBONYL)THIOSEMICARBAZIDE

Base Information

Chemical Name:4-(4-CHLOROPHENYL)-1-(4-PYRIDYLCARBONYL)THIOSEMICARBAZIDE
CAS No.:74270-72-7
Molecular Formula:C13H11ClN4OS
Molecular Weight:306.776
Hs Code.:
Mol file:74270-72-7.mol

Synonyms:4-(4-Chlor-phenyl)-1-isonicotinoyl-thiosemicarbazid;1-Isonicotinoyl-4-(4-chlor-phenyl)-thiosemicarbazid;4-(4-chloro-phenyl)-1-isonicotinoyl-thiosemicarbazide;N-isonicotinyl-N'-p-chlorophenylthiosemicarbazide;1-isonicotinoyl-4-p-chlorophenyl thiosemicarbazide;

Suppliers and Price of 4-(4-CHLOROPHENYL)-1-(4-PYRIDYLCARBONYL)THIOSEMICARBAZIDE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 4-(4-CHLOROPHENYL)-1-(4-PYRIDYLCARBONYL)THIOSEMICARBAZIDE

Chemical Property:

PSA：98.14000
LogP:3.22120

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-(4-CHLOROPHENYL)-1-(4-PYRIDYLCARBONYL)THIOSEMICARBAZIDE

There total 4 articles about 4-(4-CHLOROPHENYL)-1-(4-PYRIDYLCARBONYL)THIOSEMICARBAZIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 54-85-3,7640-37-1
isoniazid

: 2131-55-7
4-Chlorophenyl isothiocyanate

: 74270-72-7
N-(4-chlorophenyl)-2-(pyridin-4-ylcarbonyl)hydrazinecarbothioamide

Guidance literature:: In ethanol; for 1h; Reflux;
DOI:10.1248/cpb.c15-00059

Reference yield:

: 75-15-0,12122-00-8
carbon disulfide

: 54-85-3,7640-37-1
isoniazid

: 106-47-8
4-chloro-aniline

: 74270-72-7
N-(4-chlorophenyl)-2-(pyridin-4-ylcarbonyl)hydrazinecarbothioamide

Guidance literature:: carbon disulfide; 4-chloro-aniline; With potassium hydroxide; In ethanol; at 0 - 5 ℃; for 1h;

isoniazid; In ethanol; at 80 ℃; for 1h;
DOI:10.1007/s00044-014-1216-5

Reference yield:

: 1197-56-4
ammonium (4-chlorophenyl)carbamodithioate

: 74270-72-7
N-(4-chlorophenyl)-2-(pyridin-4-ylcarbonyl)hydrazinecarbothioamide

Guidance literature:: Multi-step reaction with 2 steps

1: lead(II) nitrate / water

2: ethanol / Reflux

With lead(II) nitrate; In ethanol; water;
DOI:10.14233/ajchem.2017.20481