2'-BROMO-4-METHOXY-BIPHENYL

Base Information

Chemical Name:2'-BROMO-4-METHOXY-BIPHENYL
CAS No.:74447-76-0
Molecular Formula:C13H11BrO
Molecular Weight:263.134
Hs Code.:
Mol file:74447-76-0.mol

Synonyms:2-Bromo-4-methoxybenzothiazole;2-Brom-4-methoxy-benzothiazol;4-methoxy-2'-bromobiphenyl;2-bromo-4'-methoxibiphenyl;Benzothiazole,2-bromo-4-methoxy;2'-bromo-4-methoxy-biphenyl;2-bromo-4'-methoxy-1,1'-biphenyl;

Suppliers and Price of 2'-BROMO-4-METHOXY-BIPHENYL

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 11 raw suppliers

Chemical Property of 2'-BROMO-4-METHOXY-BIPHENYL

Chemical Property:

PSA：9.23000
LogP:4.12470

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2'-BROMO-4-METHOXY-BIPHENYL

There total 24 articles about 2'-BROMO-4-METHOXY-BIPHENYL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 583-55-1
1-Bromo-2-iodobenzene

: 696-62-8
para-iodoanisole

: 74447-76-0
2-bromo-4'-methoxy-1,1'-biphenyl

Guidance literature:: para-iodoanisole; With tert.-butyl lithium; In tetrahydrofuran; at -78 ℃; for 1h;

With zinc dibromide; In tetrahydrofuran; at 20 ℃; for 0.5h;

1-Bromo-2-iodobenzene; With triphenylphosphine; [Pd(dibenzylideneacetone)2]; In tetrahydrofuran; at 20 ℃;
DOI:10.1002/chem.200400023

Reference yield: 92.0%

: 104-92-7
1-bromo-4-methoxy-benzene

: 583-55-1
1-Bromo-2-iodobenzene

: 74447-76-0
2-bromo-4'-methoxy-1,1'-biphenyl

Guidance literature:: 1-bromo-4-methoxy-benzene; With tert.-butyl lithium; In tetrahydrofuran; at -78 ℃; for 1h;

With zinc dibromide; In tetrahydrofuran; at -45 ℃;

1-Bromo-2-iodobenzene; With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; triphenylphosphine; In tetrahydrofuran; at 20 ℃;
DOI:10.3762/bjoc.10.78

Reference yield: 88.0%

: 696-62-8
para-iodoanisole

: 244205-40-1
(2-bromophenyl)boronic acid

: 74447-76-0
2-bromo-4'-methoxy-1,1'-biphenyl

Guidance literature:: With palladium diacetate; potassium carbonate; triphenylphosphine; In 1,2-dimethoxyethane; water; at 80 ℃; for 24h; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.joc.9b00598