3'-Thymidylic acid, 5'-O-[(4-methoxyphenyl)diphenylmethyl]-, mono[2-(4-nitrophenyl)ethyl] ester, compd. with N,N-diethylethanamine (1:1)

Base Information

Chemical Name:3'-Thymidylic acid, 5'-O-[(4-methoxyphenyl)diphenylmethyl]-, mono[2-(4-nitrophenyl)ethyl] ester, compd. with N,N-diethylethanamine (1:1)
CAS No.:74712-84-8
Molecular Formula:C₆H₁₅N*C₃₈H₃₈N₃O₁₁P
Molecular Weight:844.899
Hs Code.:

3'-Thymidylic acid, 5'-O-[(4-methoxyphenyl)diphenylmethyl]-,
mono[2-(4-nitrophenyl)ethyl] ester, compd. with N,N-diethylethanamine
(1:1)

Synonyms:

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Chemical Property of 3'-Thymidylic acid, 5'-O-[(4-methoxyphenyl)diphenylmethyl]-, mono[2-(4-nitrophenyl)ethyl] ester, compd. with N,N-diethylethanamine (1:1)

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Technology Process of 3'-Thymidylic acid, 5'-O-[(4-methoxyphenyl)diphenylmethyl]-, mono[2-(4-nitrophenyl)ethyl] ester, compd. with N,N-diethylethanamine (1:1)

There total 5 articles about 3'-Thymidylic acid, 5'-O-[(4-methoxyphenyl)diphenylmethyl]-, mono[2-(4-nitrophenyl)ethyl] ester, compd. with N,N-diethylethanamine (1:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 74706-78-8
(5'-O-Monomethoxytritylthymidin-3')(2,5-dichlorphenyl)(p-nitrophenylaethyl)phosphorsaeureester

: 121-44-8
triethylamine

: 74712-84-8
Triaethylammonium(5'-O-monomethoxytritylthymidin-3')(p-nitrophenylaethyl)phosphat

Guidance literature:: With 4-nitrobenzaldehyde oxime;
DOI:10.1016/S0040-4039(00)71364-5

Reference yield:

: 103-45-7
acetic acid phenethyl ester

: 74712-84-8
Triaethylammonium(5'-O-monomethoxytritylthymidin-3')(p-nitrophenylaethyl)phosphat

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) H₂SO₄, HNO₃; 2.) HCl / 1.) acetic anhydride, -15 deg C, 105 min; 2.) methanol, reflux, 3.5 h

2: pyridine / 24 h / Ambient temperature

3: 96 percent / dioxane; H₂O / 2 h / Ambient temperature

With hydrogenchloride; sulfuric acid; nitric acid; In 1,4-dioxane; pyridine; water;
DOI:10.1002/hlca.19810640547

Reference yield:

: 100-27-6
2-(4-nitrophenyl)ethanol

: 74712-84-8
Triaethylammonium(5'-O-monomethoxytritylthymidin-3')(p-nitrophenylaethyl)phosphat

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 24 h / Ambient temperature

2: 96 percent / dioxane; H₂O / 2 h / Ambient temperature

In 1,4-dioxane; pyridine; water;
DOI:10.1002/hlca.19810640547