1(3H)-Isobenzofuranone, 4-methoxy-3-(phenylsulfonyl)-

Base Information

Chemical Name:1(3H)-Isobenzofuranone, 4-methoxy-3-(phenylsulfonyl)-
CAS No.:74724-81-5
Molecular Formula:C15H12O5S
Molecular Weight:304.323
Hs Code.:
DSSTox Substance ID:DTXSID60452309
Nikkaji Number:J1.334.891J

Synonyms:74724-81-5;4-methoxy-3-(phenylsulfonyl)isobenzofuran-1(3H)-one;1(3H)-Isobenzofuranone, 4-methoxy-3-(phenylsulfonyl)-;DTXSID60452309;1-(Phenylsulfonyl)-7-methoxyisobenzofuran-3(1H)-one

Suppliers and Price of 1(3H)-Isobenzofuranone, 4-methoxy-3-(phenylsulfonyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 1(3H)-Isobenzofuranone, 4-methoxy-3-(phenylsulfonyl)-

Chemical Property:

XLogP3:2.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:3
Exact Mass:304.04054465
Heavy Atom Count:21
Complexity:489

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=CC2=C1C(OC2=O)S(=O)(=O)C3=CC=CC=C3

Technology Process of 1(3H)-Isobenzofuranone, 4-methoxy-3-(phenylsulfonyl)-

There total 9 articles about 1(3H)-Isobenzofuranone, 4-methoxy-3-(phenylsulfonyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.5%

: 107952-44-3
4-methoxy-3-phenylthioisobenzofuran-1(3H)-one

: 74724-81-5
4-methoxy-3-(phenylsulfonyl)-1-(3H)-isobenzofuranone

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 0.25h;
DOI:10.1002/1522-2675(200211)85:11<3589::AID-HLCA3589>3.0.CO;2-Z

Reference yield:

: 62924-93-0
N,N-diethyl-3-methoxybenzamide

: 74724-81-5
4-methoxy-3-(phenylsulfonyl)-1-(3H)-isobenzofuranone

Guidance literature:: Multi-step reaction with 4 steps

1: 1) s-butyllithium, tetramethylethylenediamine / 1) ether, -78 deg C, 1 h 2) ether, -78 deg C, 1 h, then to RT

2: 95 percent / 2M aq. KOH / Ambient temperature

3: 85 percent / toluene-4-sulphonic acid / benzene / Heating

4: 90 percent / 3-chloroperbenzoic acid / CH₂Cl₂ / 0 - 20 °C

With potassium hydroxide; N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; benzene;

Reference yield:

: 70946-15-5
N,N-diethyl 2-formyl-3-methoxybenzamide

: 74724-81-5
4-methoxy-3-(phenylsulfonyl)-1-(3H)-isobenzofuranone

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / 2M aq. KOH / Ambient temperature

2: 85 percent / toluene-4-sulphonic acid / benzene / Heating

3: 90 percent / 3-chloroperbenzoic acid / CH₂Cl₂ / 0 - 20 °C

With potassium hydroxide; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; benzene;