Oxetane, 3-methoxy-2-(2-phenylethyl)-, trans-

Base Information

Chemical Name:Oxetane, 3-methoxy-2-(2-phenylethyl)-, trans-
CAS No.:74824-85-4
Molecular Formula:C₁₂H₁₆O₂
Molecular Weight:192.258
Hs Code.:

Synonyms:

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Chemical Property of Oxetane, 3-methoxy-2-(2-phenylethyl)-, trans-

Chemical Property:

Purity/Quality:

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MSDS Files:: SDS file from LookChem

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Technology Process of Oxetane, 3-methoxy-2-(2-phenylethyl)-, trans-

There total 11 articles about Oxetane, 3-methoxy-2-(2-phenylethyl)-, trans- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 90878-19-6
phenethylmagnesium chloride

: 74824-85-4
(2S,3R)-3-Methoxy-2-phenethyl-oxetane

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 0 °C

2: 1) m-CPBA , 2) NaOH / 1) room temperature, 30 min, 2) room temperature, 18 h

With sodium hydroxide; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran;
DOI:10.1021/jo00181a020

Reference yield:

: 88842-06-2
Toluene-4-sulfonic acid (2S,3R)-3-hydroxy-2-methoxy-5-phenyl-pentyl ester

: 74824-85-4
(2S,3R)-3-Methoxy-2-phenethyl-oxetane

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; Ambient temperature;
DOI:10.1021/jo00181a020

Reference yield:

: 104-53-0
3-phenyl-propionaldehyde

: 74824-85-4
(2S,3R)-3-Methoxy-2-phenethyl-oxetane

Guidance literature:: Multi-step reaction with 8 steps

1: 1) lithium dicyclohexylamide / 1) -78 deg C, THF, 40 min, 2) a) -78 deg C, THF, 1h, b) room temperature, 1h

2: LiAlH₄ / diethyl ether

3: p-TsOH / tetrahydrofuran / Ambient temperature

4: tetrabutylammonium hydroxide, t-BuOOH, OsO₄ / 2-methyl-propan-2-ol / 0 °C

5: NaH / tetrahydrofuran / Ambient temperature

6: 1N HCl / Ambient temperature

7: pyridine / 0 °C

8: Potassium tert-Butylat / tetrahydrofuran / Ambient temperature

With pyridine; hydrogenchloride; tert.-butylhydroperoxide; osmium(VIII) oxide; lithium aluminium tetrahydride; potassium tert-butylate; tetra(n-butyl)ammonium hydroxide; sodium hydride; lithium dicyclohexylamide; toluene-4-sulfonic acid; In tetrahydrofuran; diethyl ether; tert-butyl alcohol;
DOI:10.1021/jo00181a020