1-Decyn-3-ol, (3S)-

Base Information

Chemical Name:1-Decyn-3-ol, (3S)-
CAS No.:74867-42-8
Molecular Formula:C10H18O
Molecular Weight:154.252
Hs Code.:
DSSTox Substance ID:DTXSID80452467
Nikkaji Number:J1.793.621B
Wikidata:Q82273122

Synonyms:1-Decyn-3-ol, (3S)-;74867-42-8;(S)-1-Decyne-3-ol;SCHEMBL9794270;DTXSID80452467

Suppliers and Price of 1-Decyn-3-ol, (3S)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 1-Decyn-3-ol, (3S)-

Chemical Property:

XLogP3:3.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:6
Exact Mass:154.135765193
Heavy Atom Count:11
Complexity:120

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCCCCC(C#C)O
Isomeric SMILES:CCCCCCC[C@@H](C#C)O

Technology Process of 1-Decyn-3-ol, (3S)-

There total 1 articles about 1-Decyn-3-ol, (3S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 74824-55-8
(S,R)-1-Ethynyloctyl N-<1-(-Naphthyl)ethyl>carbamate

: 42340-98-7
(R)-1-(1-naphthyl)ethyl isocyanate

: 74867-42-8
(-)-(S)-dec-1-yn-3-ol

Guidance literature:: With trichlorosilane; triethylamine; In dichloromethane; Yield given; Heating;
DOI:10.1021/jo01310a017

Reference yield: 47.0%

: 74867-42-8
(-)-(S)-dec-1-yn-3-ol

: 2043-61-0
cyclohexanecarbaldehyde

: (S_a,S)-1-cyclohexyl-1,2-undecadien-4-ol

Guidance literature:: With (R)-α,α-diphenylprolinol; copper(ll) bromide; In 1,4-dioxane; at 120 ℃; for 12h;
DOI:10.1002/cjoc.201800090

Reference yield:

: 74867-42-8
(-)-(S)-dec-1-yn-3-ol

: (R_a,S)-diethyl 2-(1-cyclohexylundeca-1,2-dien-4-yl)malonate

Guidance literature:: Multi-step reaction with 3 steps

1: (S)-diphenylprolinol; copper(ll) bromide / 1,4-dioxane / 12 h / 120 °C

2: triethylamine; dmap / diethyl ether / 2 h / 20 °C

3: potassium carbonate; (R)-((4,4’-bi-1,3-benzodioxole)-5,5’-diyl)bis(bis(3,5-di-t-butyl-4-methoxyphenyl))phosphine; [Pd(π-cinnamyl)Cl]₂ / 1-methyl-pyrrolidin-2-one / 12 h / 30 °C / Schlenk technique; Glovebox; Inert atmosphere

With (R)-((4,4’-bi-1,3-benzodioxole)-5,5’-diyl)bis(bis(3,5-di-t-butyl-4-methoxyphenyl))phosphine; dmap; (S)-diphenylprolinol; [Pd(π-cinnamyl)Cl]₂; potassium carbonate; triethylamine; copper(ll) bromide; In 1,4-dioxane; 1-methyl-pyrrolidin-2-one; diethyl ether;
DOI:10.1002/cjoc.201800090