N-(Chlorocyclohexylidenemethyl)-N-ethylethanamine

Base Information

Chemical Name:N-(Chlorocyclohexylidenemethyl)-N-ethylethanamine
CAS No.:75115-53-6
Molecular Formula:C₁₁H₂₀ClN
Molecular Weight:201.739
Hs Code.:
DSSTox Substance ID:DTXSID201234420

Synonyms:N-(Chlorocyclohexylidenemethyl)-N-ethylethanamine;DTXSID201234420;75115-53-6

Suppliers and Price of N-(Chlorocyclohexylidenemethyl)-N-ethylethanamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of N-(Chlorocyclohexylidenemethyl)-N-ethylethanamine

Chemical Property:

XLogP3:4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:201.1284273
Heavy Atom Count:13
Complexity:175

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCN(CC)C(=C1CCCCC1)Cl

Technology Process of N-(Chlorocyclohexylidenemethyl)-N-ethylethanamine

There total 2 articles about N-(Chlorocyclohexylidenemethyl)-N-ethylethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (Chloro-cyclohexyl-methylene)-diethyl-ammonium; chloride

: 75115-53-6
(1-chloro-cyclohexyldimethyl)diethylamine

Guidance literature:: With triethylamine; In dichloromethane; at 50 ℃; for 2h; Yield given;
DOI:10.1016/0040-4020(95)01126-9

Reference yield:

: 5461-52-9
N,N-diethylcyclohexanecarboxamide

: 75115-53-6
(1-chloro-cyclohexyldimethyl)diethylamine

Guidance literature:: Multi-step reaction with 2 steps

1: phosgene / CH₂Cl₂ / Ambient temperature

2: Et₃N / CH₂Cl₂ / 2 h / 50 °C

With phosgene; triethylamine; In dichloromethane;
DOI:10.1016/0040-4020(95)01126-9

Reference yield:

: 593-60-2,25951-54-6
Vinyl bromide

: 75115-53-6
(1-chloro-cyclohexyldimethyl)diethylamine

: (1-cyclohexylideneallyl)diethylamine

Guidance literature:: With tert.-butyl lithium; Yield given. Multistep reaction; 1.) THF, -78 deg C, 3 h, 2.) THF, from -78 deg C to RT, overnight;
DOI:10.1016/0040-4020(95)01126-9