Benzenesulfenamide, 4-chloro-N-(4-oxo-2,5-cyclohexadien-1-ylidene)-

Base Information

Chemical Name:Benzenesulfenamide, 4-chloro-N-(4-oxo-2,5-cyclohexadien-1-ylidene)-
CAS No.:75142-03-9
Molecular Formula:C12H8ClNOS
Molecular Weight:249.721
Hs Code.:
DSSTox Substance ID:DTXSID00405394

Synonyms:75142-03-9;Benzenesulfenamide, 4-chloro-N-(4-oxo-2,5-cyclohexadien-1-ylidene)-;ST50774726;DTXSID00405394;AKOS002317338

Suppliers and Price of Benzenesulfenamide, 4-chloro-N-(4-oxo-2,5-cyclohexadien-1-ylidene)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenesulfenamide, 4-chloro-N-(4-oxo-2,5-cyclohexadien-1-ylidene)-

Chemical Property:

XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:249.0015127
Heavy Atom Count:16
Complexity:336

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC(=O)C=CC1=NSC2=CC=C(C=C2)Cl

Technology Process of Benzenesulfenamide, 4-chloro-N-(4-oxo-2,5-cyclohexadien-1-ylidene)-

There total 4 articles about Benzenesulfenamide, 4-chloro-N-(4-oxo-2,5-cyclohexadien-1-ylidene)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

: 123-30-8
4-amino-phenol

: 75141-99-0
p-chlorophenyl thionitrate

: 75142-03-9
N-<(p-chlorophenyl)thio>-1,4-benzoquinone 4-imine

Guidance literature:: In acetonitrile; for 1h; Ambient temperature;
DOI:10.1246/bcsj.53.775

Reference yield:

: 1142-19-4
4,4'-dichlorodiphenyl disulfide

: 75142-03-9
N-<(p-chlorophenyl)thio>-1,4-benzoquinone 4-imine

Guidance literature:: Multi-step reaction with 2 steps

1: Cl₂ / CCl₄ / 0 °C

2: benzene; pyridine / 0.67 h / Ambient temperature

With chlorine; In pyridine; tetrachloromethane; benzene;
DOI:10.1021/jo00317a011

Reference yield:

: 106-54-7
p-Chlorothiophenol

: 75142-03-9
N-<(p-chlorophenyl)thio>-1,4-benzoquinone 4-imine

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / N₂O₄ / CCl₄; hexane / 0.08 h / -60 °C

2: 18 percent / acetonitrile / 1 h / Ambient temperature

With dinitrogen tetraoxide; In tetrachloromethane; hexane; acetonitrile;
DOI:10.1246/bcsj.53.775