2-amino-3-hydroxy-4,6-dimethyl-7-oxo-N,N-bis(7,11,14-trimethyl-2,5,9,12,15-pentaoxo-3,10-dipropan-2-yl-8-oxa-1,4,11,14-tetrazabicyclo[14.3.0]nonadec-6-yl)phenoxazine-1,9-dicarboxamide

Base Information

• Chemical Name: 2-amino-3-hydroxy-4,6-dimethyl-7-oxo-N,N-bis(7,11,14-trimethyl-2,5,9,12,15-pentaoxo-3,10-dipropan-2-yl-8-oxa-1,4,11,14-tetrazabicyclo[14.3.0]nonadec-6-yl)phenoxazine-1,9-dicarboxamide
• CAS No.: 21478-73-9
• Molecular Formula: C62H86N12O17
• Molecular Weight: 1271.4164

Synonyms:

Chemical Property of 2-amino-3-hydroxy-4,6-dimethyl-7-oxo-N,N-bis(7,11,14-trimethyl-2,5,9,12,15-pentaoxo-3,10-dipropan-2-yl-8-oxa-1,4,11,14-tetrazabicyclo[14.3.0]nonadec-6-yl)phenoxazine-1,9-dicarboxamide

Chemical Property:

• Boiling Point: 1402.8°Cat760mmHg
• Flash Point: 802.2°C
• Density: 1.44g/cm³

Purity/Quality:

Safty Information:

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Useful:

Technology Process of 2-amino-3-hydroxy-4,6-dimethyl-7-oxo-N,N-bis(7,11,14-trimethyl-2,5,9,12,15-pentaoxo-3,10-dipropan-2-yl-8-oxa-1,4,11,14-tetrazabicyclo[14.3.0]nonadec-6-yl)phenoxazine-1,9-dicarboxamide

There total 1 articles about 2-amino-3-hydroxy-4,6-dimethyl-7-oxo-N,N-bis(7,11,14-trimethyl-2,5,9,12,15-pentaoxo-3,10-dipropan-2-yl-8-oxa-1,4,11,14-tetrazabicyclo[14.3.0]nonadec-6-yl)phenoxazine-1,9-dicarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

C70H90N12O17 (70570-56-8) → 7-hydroxyactinomycin D (21478-73-9) + 2-phenyl-9,11-dimethyl-8-oxooxazolo<4,5-b>phenoxazine 4,6-bis lactone (87039-87-0)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In methanol; for 1h; Heating;

DOI:10.1021/jm00365a015

Reference yield: 42.8%

7-hydroxyactinomycin D (21478-73-9) + 1,2-Epoxy-3-bromopropane (3132-64-7,82584-73-4) → 7-(2,3-epoxypropoxy)actinomycin D (82830-18-0,114715-30-9,114715-31-0) + 7-(2,3-dihydroxypropoxy)actinomycin D (82830-19-1,114715-22-9,114715-23-0)

Guidance literature:

With potassium carbonate; In acetone; at 50 - 55 ℃; for 16h;

DOI:10.1021/jm00352a023

Reference yield:

(R)-methoxytrifluoromethylphenylacetyl chloride (20445-33-4,39637-99-5) + 7-hydroxyactinomycin D (21478-73-9) + methyl (S)-β-bromolactate → C85H106F6N12O23 (114635-31-3) + C85H106F6N12O23 (114715-32-1)

Guidance literature:

Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;

DOI:10.1021/jm00403a010

upstream raw materials:

C₇₀H₉₀N₁₂O₁₇

Downstream raw materials:

7-(2,3-epoxypropoxy)actinomycin D

7-(2,3-dihydroxypropoxy)actinomycin D

C₈₅H₁₀₆F₆N₁₂O₂₃

C₈₅H₁₀₆F₆N₁₂O₂₃

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