Di(2-butenyl)zinc

Base Information

Chemical Name:Di(2-butenyl)zinc
CAS No.:7544-41-4
Molecular Formula:C₈H₁₄Zn
Molecular Weight:175.589
Hs Code.:
Mol file:7544-41-4.mol

Synonyms:3-Methyl-5-aethyl-anilin;3-Aethyl-5-methyl-anilin;

Suppliers and Price of Di(2-butenyl)zinc

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Di(2-butenyl)zinc

Chemical Property:

PSA：0.00000
LogP:3.05770

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Di(2-butenyl)zinc

There total 4 articles about Di(2-butenyl)zinc which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 21969-32-4
crotylmagnesium chloride

: 7646-85-7,24359-56-6
zinc(II) chloride

: 7544-41-4,80534-81-2
bis(but-2-enyl)zinc

Guidance literature:: In diethyl ether; byproducts: MgCl2; into ether soln. added ZnCl2 at 25°C for 3 h, filtered, solvent evapd.; distd. at 40°C/0.0001 Torr, elem. anal., identified by 1H-NMR;
DOI:10.1016/S0022-328X(00)81022-0

Reference yield: 91.0%

: 21969-32-4,6088-88-6
(1-methylallyl)magnesium chloride

: 7646-85-7,24359-56-6
zinc(II) chloride

: 80534-81-2,7544-41-4
Bis(2-methylprop-2-enyl)zink

Guidance literature:: In diethyl ether; byproducts: MgCl2; to ether soln. added ZnCl2 at 20°C for 1 h, MgCl2 filtered, solvent evapd.; sublimed at 40-50°C/0.0001 Torr, identified by 1H-NMR;
DOI:10.1016/S0022-328X(00)81022-0

Reference yield:

: 591-51-5
phenyllithium

: 80603-50-5
2-butenylzinc chloride

: 1078-58-6
diphenylzinc

: 7544-41-4,80534-81-2
bis(but-2-enyl)zinc

Guidance literature:: In diethyl ether; byproducts: LiCl; to soln. of MeCHCHCH2ZnCl in Et2O added soln. of PhLi in Et2O at -10 °C; filtered, evapd. (20 °C, 0.1 Torr), distd. at 37-40 (0.0001 Torr), then sublimed at 70 .gedree.C (0.0001 Torr); elem. anal.;
DOI:10.1016/0022-328X(85)88021-9