Benzamide, 3,4-dichloro-N-methyl-N-[2-(methylamino)cyclohexyl]-

Base Information

Chemical Name:Benzamide, 3,4-dichloro-N-methyl-N-[2-(methylamino)cyclohexyl]-
CAS No.:75570-61-5
Molecular Formula:C15H20Cl2N2O
Molecular Weight:315.243
Hs Code.:

Synonyms:

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Chemical Property of Benzamide, 3,4-dichloro-N-methyl-N-[2-(methylamino)cyclohexyl]-

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Technology Process of Benzamide, 3,4-dichloro-N-methyl-N-[2-(methylamino)cyclohexyl]-

There total 4 articles about Benzamide, 3,4-dichloro-N-methyl-N-[2-(methylamino)cyclohexyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3,4-dichloro-N-(2-(dimethylamino)cyclohexyl)-N-methylbenzamide

: 75570-61-5
N-methyl-N-[2-(N'-methylamino)cyclohexyl]-3,4-dichlorobenzamide

Guidance literature:: 3,4-dichloro-N-(2-(dimethylamino)cyclohexyl)-N-methylbenzamide; With carbonochloridic acid 1-chloro-ethyl ester; In 1,2-dichloro-ethane; at 0 ℃; Inert atmosphere; Reflux;

With methanol; at 60 ℃; for 6h; Inert atmosphere;

Reference yield:

: 67198-26-9
trans-N,N-dimethyl-N-methyl-1,2-cyclohexanediamine

: 75570-61-5
N-methyl-N-[2-(N'-methylamino)cyclohexyl]-3,4-dichlorobenzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

2.1: carbonochloridic acid 1-chloro-ethyl ester / 1,2-dichloro-ethane / 0 °C / Inert atmosphere; Reflux

2.2: 6 h / 60 °C / Inert atmosphere

With carbonochloridic acid 1-chloro-ethyl ester; triethylamine; In tetrahydrofuran; 1,2-dichloro-ethane;

Reference yield:

: 3024-72-4
3,4-dichlorobenzoyl chloride

: 75570-61-5
N-methyl-N-[2-(N'-methylamino)cyclohexyl]-3,4-dichlorobenzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

2.1: carbonochloridic acid 1-chloro-ethyl ester / 1,2-dichloro-ethane / 0 °C / Inert atmosphere; Reflux

2.2: 6 h / 60 °C / Inert atmosphere

With carbonochloridic acid 1-chloro-ethyl ester; triethylamine; In tetrahydrofuran; 1,2-dichloro-ethane;