4-Amino-N-(3-hydroxyphenyl)benzene-1-sulfonamide

Base Information

• Chemical Name: 4-Amino-N-(3-hydroxyphenyl)benzene-1-sulfonamide
• CAS No.: 75762-45-7
• Molecular Formula: C₁₂H₁₂N₂O₃S
• Molecular Weight: 264.305
• DSSTox Substance ID: DTXSID20552657
• Wikidata: Q82433015

Synonyms:75762-45-7;4-Amino-N-(3-hydroxyphenyl)benzene-1-sulfonamide;SCHEMBL8864887;DTXSID20552657;AKOS010414182

Chemical Property of 4-Amino-N-(3-hydroxyphenyl)benzene-1-sulfonamide

Chemical Property:

• XLogP3: 1.2
• Hydrogen Bond Donor Count: 3
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 3
• Exact Mass: 264.05686342
• Heavy Atom Count: 18
• Complexity: 358

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=CC(=C1)O)NS(=O)(=O)C2=CC=C(C=C2)N

Technology Process of 4-Amino-N-(3-hydroxyphenyl)benzene-1-sulfonamide

There total 6 articles about 4-Amino-N-(3-hydroxyphenyl)benzene-1-sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-acetylaminobenzenesulfonyl chloride (121-60-8) → sulfanilic acid-(3-hydroxy-anilide) (75762-45-7)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine

2: aq. NaOH solution

With pyridine; sodium hydroxide;

Reference yield:

N-acetyl-sulfanilic acid-(3-hydroxy-anilide) (405296-03-9) → sulfanilic acid-(3-hydroxy-anilide) (75762-45-7)

Guidance literature:

With hydrogenchloride;

DOI:10.1021/ja01274a009

Reference yield:

m-Hydroxyaniline (591-27-5) → sulfanilic acid-(3-hydroxy-anilide) (75762-45-7)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine

2: aq. NaOH solution

With pyridine; sodium hydroxide;

upstream raw materials:

N-acetyl-sulfanilic acid-(3-hydroxy-anilide)

m-Hydroxyaniline

p-acetylaminobenzenesulfonyl chloride

N-{4-[(3-nitrophenyl)sulfamoyl]phenyl}acetamide

Downstream raw materials:

N-(3-Hydroxy-phenyl)-4-(8-hydroxy-quinolin-5-ylazo)-benzenesulfonamide

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