2,5-dimethoxybicyclo[4.2.0]octa-1,3,5-triene-7,8-dione

Base Information

Chemical Name:2,5-dimethoxybicyclo[4.2.0]octa-1,3,5-triene-7,8-dione
CAS No.:75833-47-5
Molecular Formula:C₁₀H₈O₄
Molecular Weight:192.171
Hs Code.:

Synonyms:3,6-Dimethoxy-1,2-benzocyclobutendion;3,6-dimethoxybenzocyclobutenedione;2,5-Dimethoxy-bicyclo[4.2.0]octa-1,3,5-triene-7,8-dione;

Suppliers and Price of 2,5-dimethoxybicyclo[4.2.0]octa-1,3,5-triene-7,8-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2,5-DIMETHOXYBICYCLO[4.2.0]OCTA-1,3,5-TRIENE-7,8-DIONE 95.00%
5MG
$ 505.80

Total 1 raw suppliers

Chemical Property of 2,5-dimethoxybicyclo[4.2.0]octa-1,3,5-triene-7,8-dione

Chemical Property:

Melting Point:190 - 192 °C (cyclohexane)
PSA：52.60000
LogP:0.45300

Purity/Quality:

99% ^*data from raw suppliers

2,5-DIMETHOXYBICYCLO[4.2.0]OCTA-1,3,5-TRIENE-7,8-DIONE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,5-dimethoxybicyclo[4.2.0]octa-1,3,5-triene-7,8-dione

There total 4 articles about 2,5-dimethoxybicyclo[4.2.0]octa-1,3,5-triene-7,8-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 75833-46-4
2,2-dibromo-3,6-dimethoxybenzocyclobuten-1(2H)-one

: 75833-47-5
3,6-dimethoxybenzocyclobutene-1,2-dione

Guidance literature:: With silver trifluoroacetate; In acetonitrile; for 4h; Heating; protection from light;

Reference yield:

: 75833-45-3
2,5-dimethoxybicyclo[4.2.0]octa-1,3,5-trien-7-one

: 75833-47-5
3,6-dimethoxybenzocyclobutene-1,2-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / N-bromosuccinimide, benzoyl peroxide / CCl₄ / 4 h / Heating

2: 94 percent / silver trifluoroacetate / acetonitrile / 4 h / Heating; protection from light

With N-Bromosuccinimide; Perbenzoic acid; silver trifluoroacetate; In tetrachloromethane; acetonitrile;