6-Ethoxy-benzo[1,3]dioxole-5-carbaldehyde

Base Information

Chemical Name:6-Ethoxy-benzo[1,3]dioxole-5-carbaldehyde
CAS No.:75889-50-8
Molecular Formula:C10H10O4
Molecular Weight:194.18400
Hs Code.:2932999099
DSSTox Substance ID:DTXSID00390019
Wikidata:Q82186384
Mol file:75889-50-8.mol

Synonyms:75889-50-8;6-Ethoxy-benzo[1,3]dioxole-5-carbaldehyde;6-Ethoxybenzo[d][1,3]dioxole-5-carbaldehyde;6-ethoxy-1,3-benzodioxole-5-carbaldehyde;DTXSID00390019;AKOS000103737;CS-0455576

Suppliers and Price of 6-Ethoxy-benzo[1,3]dioxole-5-carbaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
6-Ethoxy-benzo[1,3]dioxole-5-carbaldehyde
500mg
$ 188.00

Matrix Scientific
6-Ethoxy-benzo[1,3]dioxole-5-carbaldehyde
1g
$ 308.00

Crysdot
6-Ethoxybenzo[d][1,3]dioxole-5-carbaldehyde 97%
5g
$ 874.00

American Custom Chemicals Corporation
6-ETHOXY-BENZO[1,3]DIOXOLE-5-CARBALDEHYDE 95.00%
500MG
$ 777.32

AK Scientific
6-Ethoxy-benzo[1,3]dioxole-5-carbaldehyde
500mg
$ 303.00

Total 3 raw suppliers

Chemical Property of 6-Ethoxy-benzo[1,3]dioxole-5-carbaldehyde

Chemical Property:

PSA：44.76000
LogP:1.62650
XLogP3:1.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:194.05790880
Heavy Atom Count:14
Complexity:206

Purity/Quality:

97% ^*data from raw suppliers

6-Ethoxy-benzo[1,3]dioxole-5-carbaldehyde ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:Xi

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC1=CC2=C(C=C1C=O)OCO2

Technology Process of 6-Ethoxy-benzo[1,3]dioxole-5-carbaldehyde

There total 3 articles about 6-Ethoxy-benzo[1,3]dioxole-5-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 533-31-3
Sesamol

: 75889-50-8
6-ethoxypiperonal

Guidance literature:: Multi-step reaction with 3 steps

1: 52 percent / KOH / H₂O; methanol / 48 h / Ambient temperature

2: 41 percent / Br₂ / CCl₄ / 2 h / 0 °C

3: 1.) 1.6 M n-BuLi in hexanes / 1.) ether, -78 deg C, 10 min, 2.) from -78 deg C to RT, 30 min

With potassium hydroxide; n-butyllithium; bromine; In methanol; tetrachloromethane; water;
DOI:10.1021/jm00084a011

Reference yield:

: 87590-41-8
sesamylethyl ether

: 75889-50-8
6-ethoxypiperonal

Guidance literature:: Multi-step reaction with 2 steps

1: 41 percent / Br₂ / CCl₄ / 2 h / 0 °C

2: 1.) 1.6 M n-BuLi in hexanes / 1.) ether, -78 deg C, 10 min, 2.) from -78 deg C to RT, 30 min

With n-butyllithium; bromine; In tetrachloromethane;
DOI:10.1021/jm00084a011

Reference yield:

: 118280-62-9
5-bromo-6-ethoxy-1,3-benzodioxole

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 75889-50-8
6-ethoxypiperonal

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction; 1.) ether, -78 deg C, 10 min, 2.) from -78 deg C to RT, 30 min;
DOI:10.1021/jm00084a011