Technology Process of 24-Hydroxytetracosanoic acid
There total 16 articles about 24-Hydroxytetracosanoic acid which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
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Multi-step reaction with 4 steps
1: 100 percent / 15 h / 140 °C
2: 1.) NaN(SiCH3)2 / 1.) THF, a) r.t., 30 min., b) reflux, 1 h, 2.) THF, a) 0 deg C, 1 h, b) r.t., 15 h
3: 97 percent / H2 / 10percent Pd/C / ethyl acetate
4: 95 percent / NaOH / methanol / 20 h / Heating
With
sodium hydroxide; hydrogen; sodium hexamethyldisilazane;
palladium on activated charcoal;
In
methanol; ethyl acetate;
DOI:10.1002/hlca.19930760141
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 87 percent / pyridinium chlorochromate / CH2Cl2 / 2.5 h / Ambient temperature
2: 1.) NaN(SiCH3)2 / 1.) THF, a) r.t., 30 min., b) reflux, 1 h, 2.) THF, a) 0 deg C, 1 h, b) r.t., 15 h
3: 97 percent / H2 / 10percent Pd/C / ethyl acetate
4: 95 percent / NaOH / methanol / 20 h / Heating
With
sodium hydroxide; hydrogen; sodium hexamethyldisilazane; pyridinium chlorochromate;
palladium on activated charcoal;
In
methanol; dichloromethane; ethyl acetate;
DOI:10.1002/hlca.19930760141
