Aluminum, hexylbis(2-methylpropyl)-

Base Information

Chemical Name:Aluminum, hexylbis(2-methylpropyl)-
CAS No.:75925-84-7
Molecular Formula:C14H31Al
Molecular Weight:226.382
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Aluminum, hexylbis(2-methylpropyl)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of Aluminum, hexylbis(2-methylpropyl)-

There total 4 articles about Aluminum, hexylbis(2-methylpropyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 592-41-6,25067-06-5
1-hexene

: 1779-25-5
diisobutylaluminum chloride

: 893417-73-7
i-Bu(Cl)AlC₆H₁₃

: 75925-84-7
(i-Bu)2AlC₆H₁₃

Guidance literature:: zirconocene dichloride; In benzene; (Ar); mixture of Zr complex, olefine and soln. of organoaluminum compd. diluted with benzene, stirred at 20 °C for 5 h;
DOI:10.1007/s11172-005-0254-z

Reference yield:

: n-hexylzirconocene chloride

: 1779-25-5
diisobutylaluminum chloride

: 1291-32-3
zirconocene dichloride

: 75925-84-7
(i-Bu)2AlC₆H₁₃

Guidance literature:: In ⁽²⁾H₈-toluene; (Ar); to Zr complex in toluene-d8 soln. of organoaluminum compd. added dropwise; not isolated, by NMR;
DOI:10.1007/s11172-005-0254-z

Reference yield:

: 14343-59-0
1,1-bis(diisobutylaluminium)hexane

: 108-39-4
3-methyl-phenol

: (((CH₃)2CHCH₂)2Al)CH((CH₂)4CH₃)Al(CH₂CH(CH₃)2)OC₆H₄CH₃

: 75925-84-7
(i-Bu)2AlC₆H₁₃

Guidance literature:: In toluene; byproducts: isobutane, m-MeC6H4OAl(i-Bu)2, isobutene; m-MeC6H4OH was added as slowly as possible to a soln. of alane (1:1 molar ratio) in xylene at -70°C under N2 atmosphere, mixt. was allowed to warm slowly to room temp. (IR monitoring of the progress of the reation); volume of gas evolved was measured in a gas burette, then analysed by GLC, reaction mixt. was deuterolyzed (D2O followed by 10% DCl in D2O) and analyzed by means of GLC/MS;
DOI:10.1016/0022-328X(87)80320-0