6-Amino-2-(4-chlorophenyl)-1,2,4-benzotriazin-3(2H)-one

Base Information

Chemical Name:6-Amino-2-(4-chlorophenyl)-1,2,4-benzotriazin-3(2H)-one
CAS No.:75953-52-5
Molecular Formula:C₁₃H₉ClN₄O
Molecular Weight:272.694
Hs Code.:
DSSTox Substance ID:DTXSID90504906
Wikidata:Q82359684

Synonyms:6-Amino-2-(4-chlorophenyl)-1,2,4-benzotriazin-3(2H)-one;75953-52-5;DTXSID90504906;AKOS030211153

Suppliers and Price of 6-Amino-2-(4-chlorophenyl)-1,2,4-benzotriazin-3(2H)-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 6-Amino-2-(4-chlorophenyl)-1,2,4-benzotriazin-3(2H)-one

Chemical Property:

XLogP3:1.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:272.0464886
Heavy Atom Count:19
Complexity:527

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC(=CC=C1N2C(=O)N=C3C=C(C=CC3=N2)N)Cl

Technology Process of 6-Amino-2-(4-chlorophenyl)-1,2,4-benzotriazin-3(2H)-one

There total 8 articles about 6-Amino-2-(4-chlorophenyl)-1,2,4-benzotriazin-3(2H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 105798-25-2
[5-Amino-2-(4-chloro-phenylazo)-phenyl]-carbamic acid ethyl ester

: 75953-52-5
6-Amino-2-(4-chloro-phenyl)-2H-benzo[1,2,4]triazin-3-one

Guidance literature:: With hydrogenchloride; In water; for 5h; Yield given; Heating;

Reference yield:

: 6275-72-5
ethyl N-(m-nitrophenyl)carbamate

: 75953-52-5
6-Amino-2-(4-chloro-phenyl)-2H-benzo[1,2,4]triazin-3-one

Guidance literature:: Multi-step reaction with 4 steps

1: 1) Fe-powder, 37percent HCl, 2) 34 percent anh. HCl / 1) EtOH, 30 min, reflux, 2) EtOH

2: AcONa / acetic acid; H₂O / 48 h / 0 - 3 °C

3: 3percent aq. Na₂CO₃ / 96 h / Ambient temperature

4: 37percent HCl / H₂O / 5 h / Heating

With hydrogenchloride; sodium acetate; iron; sodium carbonate; In water; acetic acid;

Reference yield:

: 122712-58-7
3-Amino-phenylcarbaminsaeureethylester-Hydrochlorid

: 75953-52-5
6-Amino-2-(4-chloro-phenyl)-2H-benzo[1,2,4]triazin-3-one

Guidance literature:: Multi-step reaction with 3 steps

1: AcONa / acetic acid; H₂O / 48 h / 0 - 3 °C

2: 3percent aq. Na₂CO₃ / 96 h / Ambient temperature

3: 37percent HCl / H₂O / 5 h / Heating

With hydrogenchloride; sodium acetate; sodium carbonate; In water; acetic acid;