Azulene, 1,2,3,5,6,7,8,8a-octahydro-1,4-dimethyl-7-(1-methylethylidene)-, cis-

Base Information

Chemical Name:Azulene, 1,2,3,5,6,7,8,8a-octahydro-1,4-dimethyl-7-(1-methylethylidene)-, cis-
CAS No.:76036-00-5
Molecular Formula:C15H24
Molecular Weight:
Hs Code.:

Synonyms:

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Chemical Property of Azulene, 1,2,3,5,6,7,8,8a-octahydro-1,4-dimethyl-7-(1-methylethylidene)-, cis-

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of Azulene, 1,2,3,5,6,7,8,8a-octahydro-1,4-dimethyl-7-(1-methylethylidene)-, cis-

There total 51 articles about Azulene, 1,2,3,5,6,7,8,8a-octahydro-1,4-dimethyl-7-(1-methylethylidene)-, cis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 59822-10-5
(+/-)-5-bromo-3-methyl-1-pentene

: 3772-93-8,31756-35-1,76036-00-5,97233-31-3
(+/-)-β-bulnesene

Guidance literature:: Multi-step reaction with 10 steps

1: 80 percent / Mg

2: m-chloroperoxybenzoic acid / CH₂Cl₂

3: pyridine

4: acetonitrile / 20 h / 150 °C

5: 73 percent / H₂ / 5percent Pd-C / ethanol

6: 77 percent

7: SOCl₂, HMPA

8: 76 percent / Na / diethyl ether / Ambient temperature

9: 70 percent / CrO₃ / pyridine

With chromium(VI) oxide; N,N,N,N,N,N-hexamethylphosphoric triamide; thionyl chloride; hydrogen; sodium; magnesium; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; In pyridine; diethyl ether; ethanol; dichloromethane; acetonitrile;
DOI:10.1039/c39830000666

Reference yield:

: 59822-10-5
(+/-)-5-bromo-3-methyl-1-pentene

: 3772-93-8,31756-35-1,76036-00-5,97233-31-3
(+/-)-4-epi-β-bulnesene

Guidance literature:: Multi-step reaction with 10 steps

1: 80 percent / Mg

2: m-chloroperoxybenzoic acid / CH₂Cl₂

3: pyridine

4: acetonitrile / 20 h / 150 °C

5: 73 percent / H₂ / 5percent Pd-C / ethanol

6: 77 percent

7: SOCl₂, HMPA

8: 76 percent / Na / diethyl ether / Ambient temperature

9: 70 percent / CrO₃ / pyridine

With chromium(VI) oxide; N,N,N,N,N,N-hexamethylphosphoric triamide; thionyl chloride; hydrogen; sodium; magnesium; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; In pyridine; diethyl ether; ethanol; dichloromethane; acetonitrile;
DOI:10.1039/c39830000666

Reference yield:

: 88125-61-5,88125-74-0
2-(1-hydroxy-4-methylhex-5-enyl)furan

: 3772-93-8,31756-35-1,76036-00-5,97233-31-3
(+/-)-β-bulnesene

Guidance literature:: Multi-step reaction with 9 steps

1: m-chloroperoxybenzoic acid / CH₂Cl₂

2: pyridine

3: acetonitrile / 20 h / 150 °C

4: 73 percent / H₂ / 5percent Pd-C / ethanol

5: 77 percent

6: SOCl₂, HMPA

7: 76 percent / Na / diethyl ether / Ambient temperature

8: 70 percent / CrO₃ / pyridine

With chromium(VI) oxide; N,N,N,N,N,N-hexamethylphosphoric triamide; thionyl chloride; hydrogen; sodium; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; In pyridine; diethyl ether; ethanol; dichloromethane; acetonitrile;
DOI:10.1039/c39830000666