3-(Trimethylstannyl)but-3-en-1-ol

Base Information

Chemical Name:3-(Trimethylstannyl)but-3-en-1-ol
CAS No.:76077-30-0
Molecular Formula:C7H16OSn
Molecular Weight:234.913
Hs Code.:
DSSTox Substance ID:DTXSID90513992
Wikidata:Q82374056

Synonyms:76077-30-0;3-(Trimethylstannyl)but-3-en-1-ol;DTXSID90513992

Suppliers and Price of 3-(Trimethylstannyl)but-3-en-1-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(Trimethylstannyl)but-3-en-1-ol

Chemical Property:

Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:236.022318
Heavy Atom Count:9
Complexity:102

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C[Sn](C)(C)C(=C)CCO

Technology Process of 3-(Trimethylstannyl)but-3-en-1-ol

There total 1 articles about 3-(Trimethylstannyl)but-3-en-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 89041-25-8
(trimethylstannyl)copper(I)*dimethyl sulfide

: 927-74-2
3-Butyn-1-ol

: 126655-31-0,76077-23-1,76077-09-3
(E)-4-trimethylstannyl-3-buten-1-ol

: 76077-30-0
3-trimethylstannyl-3-buten-1-ol

: 661-69-8
hexamethyldistannane

Guidance literature:: With ammonium chloride; In tetrahydrofuran; methanol; water; To a stirred soln. of Me3SnCu*Me2S in THF (Ar, -78°C) was added sequentially a THF soln. of the 1-alkyne and CH3OH. The mixt. was stirred(10 min) and then at -63°C (12 h). Satd. aq. NH4Cl and ether were added; allowed to warm to room temp.; Aq. phase was extd. (ether). The org. exts. were washed (satd. aq. NH4Cl) and dried (MgSO4). Removal of the solvent; flash chromy. (silica gel) gave 3-trimethylstannyl-3-buten-1-ol and (E)-4-trimethylstannyl-3-buten-1-ol.;