Indeno[1,2-c]pyrazole, 1-[bis(4-methoxyphenyl)methyl]-1,4-dihydro-6,7-dimethoxy-3-[4-(4,4,5,5 -tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-

Base Information

• Chemical Name: Indeno[1,2-c]pyrazole, 1-[bis(4-methoxyphenyl)methyl]-1,4-dihydro-6,7-dimethoxy-3-[4-(4,4,5,5 -tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-
• CAS No.: 760992-14-1
• Molecular Formula: C39H41BN2O6
• Molecular Weight: 644.575
• Mol file: 760992-14-1.mol

Synonyms:

Chemical Property of Indeno[1,2-c]pyrazole, 1-[bis(4-methoxyphenyl)methyl]-1,4-dihydro-6,7-dimethoxy-3-[4-(4,4,5,5 -tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Indeno[1,2-c]pyrazole, 1-[bis(4-methoxyphenyl)methyl]-1,4-dihydro-6,7-dimethoxy-3-[4-(4,4,5,5 -tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-

There total 1 articles about Indeno[1,2-c]pyrazole, 1-[bis(4-methoxyphenyl)methyl]-1,4-dihydro-6,7-dimethoxy-3-[4-(4,4,5,5 -tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

1-[bis(4-methoxyphenyl)methyl]-3-(4-bromophenyl)-6,7-dimethoxy-1,4-dihydroindeno[1,2-c]pyrazole (760992-13-0) + bis(pinacolato)diborane (10221-56-4) → 1-[bis(4-methoxyphenyl)methyl]-6,7-dimethoxy-3-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,4-dihydroindeno[1,2-c]pyrazole (760992-14-1)

Guidance literature:

With potassium acetate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; 1,1'-bis(diphenylphosphino)ferrocene; In 1,4-dioxane; at 90 ℃;

Reference yield: 65.0%

1-[bis(4-methoxyphenyl)methyl]-4-iodo-1H-pyrazole (760992-12-9) + 1-[bis(4-methoxyphenyl)methyl]-6,7-dimethoxy-3-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-1,4-dihydroindeno[1,2-c]pyrazole (760992-14-1) → 1-[bis(4-methoxyphenyl)methyl]-3-(4-{1-[bis(4-methoxyphenyl)methyl]-1H-pyrazol-4-yl}phenyl)-6,7-dimethoxy-1,4-dihydroindeno[1,2-c]pyrazole (760992-15-2)

Guidance literature:

With sodium carbonate; bis-triphenylphosphine-palladium(II) chloride; In 1,2-dimethoxyethane; ethanol; water; at 160 ℃; for 0.277778h; Smith Synthesizer;

upstream raw materials:

1-[bis(4-methoxyphenyl)methyl]-3-(4-bromophenyl)-6,7-dimethoxy-1,4-dihydroindeno[1,2-c]pyrazole

bis(pinacolato)diborane

Downstream raw materials:

1-[bis(4-methoxyphenyl)methyl]-3-(4-{1-[bis(4-methoxyphenyl)methyl]-1H-pyrazol-4-yl}phenyl)-6,7-dimethoxy-1,4-dihydroindeno[1,2-c]pyrazole