2-[(E)-(4-Methoxyphenyl)diazenyl]-4-methyl-3-phenyl-4H-1,4-benzothiazine

Base Information

Chemical Name:2-[(E)-(4-Methoxyphenyl)diazenyl]-4-methyl-3-phenyl-4H-1,4-benzothiazine
CAS No.:76148-77-1
Molecular Formula:C22H19N3OS
Molecular Weight:373.478
Hs Code.:
DSSTox Substance ID:DTXSID60507141

Synonyms:76148-77-1;DTXSID60507141;2-[(E)-(4-Methoxyphenyl)diazenyl]-4-methyl-3-phenyl-4H-1,4-benzothiazine

Suppliers and Price of 2-[(E)-(4-Methoxyphenyl)diazenyl]-4-methyl-3-phenyl-4H-1,4-benzothiazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 2-[(E)-(4-Methoxyphenyl)diazenyl]-4-methyl-3-phenyl-4H-1,4-benzothiazine

Chemical Property:

XLogP3:5.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:4
Exact Mass:373.12488341
Heavy Atom Count:27
Complexity:550

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN1C2=CC=CC=C2SC(=C1C3=CC=CC=C3)N=NC4=CC=C(C=C4)OC

Technology Process of 2-[(E)-(4-Methoxyphenyl)diazenyl]-4-methyl-3-phenyl-4H-1,4-benzothiazine

There total 4 articles about 2-[(E)-(4-Methoxyphenyl)diazenyl]-4-methyl-3-phenyl-4H-1,4-benzothiazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 59255-04-8
1-bromo-2-phenylglyoxal 1-(p-methoxyphenyl)hydrazone

: 21749-63-3
2-(methylamino)benzenethiol

: 76148-77-1
2-(p-methoxyphenylazo)-4-methyl-3-phenyl-4H-1,4-benzothiazine

Guidance literature:: With sodium ethanolate; In ethanol;

Reference yield:

: 16222-10-9
1-phenyl-2-(phenylthio)ethanone

: 76148-77-1
2-(p-methoxyphenylazo)-4-methyl-3-phenyl-4H-1,4-benzothiazine

Guidance literature:: Multi-step reaction with 3 steps

1: KBr / H₂O / 0.5 h / 100 °C

2: 76 percent / sodium acetate / H₂O; methanol

3: 94 percent / sodium ethoxide / ethanol

With sodium ethanolate; sodium acetate; potassium bromide; In methanol; ethanol; water;

Reference yield:

: p-methoxybenzene diazonium sulphate

: 76148-77-1
2-(p-methoxyphenylazo)-4-methyl-3-phenyl-4H-1,4-benzothiazine

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / sodium acetate / H₂O; methanol

2: 94 percent / sodium ethoxide / ethanol

With sodium ethanolate; sodium acetate; In methanol; ethanol; water;