CRYPTHOPHANE E

Base Information

• Chemical Name: CRYPTHOPHANE E
• CAS No.: 102683-14-7
• Molecular Formula: C₅₇H₆₀O₁₂
• Molecular Weight: 937.096
• Mol file: 102683-14-7.mol

Synonyms:(?à)-Cryptophane E; Cryptophane 333;Cryptophane E

Chemical Property of CRYPTHOPHANE E

Chemical Property:

• Melting Point: >260°C
• Refractive Index: 1.6390 (estimate)
• Boiling Point: 731.58°C (rough estimate)
• PSA: 110.76000
• Density: 1.0827 (rough estimate)
• LogP: 9.69660

Purity/Quality:

99% ^*data from raw suppliers

CRYPTHOPHANE E 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of CRYPTHOPHANE E

There total 11 articles about CRYPTHOPHANE E which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

(rac)-2,7,12-tris<3-<4-(hydroxymethyl)-2-methoxyphenoxy>propoxy>-3,8,13-trimethoxy-10,15-dihydro-5H-tribenzocyclononene → cryptophane-E (102683-14-7,102735-01-3,110352-20-0,155322-30-8) + cryptophane F (102683-15-8)

Guidance literature:

With formic acid; In chloroform; at 60 ℃; for 3h;

DOI:10.1021/ja00255a035

Reference yield: 50.0%

[4-(3-{7,12-Bis-[3-(4-hydroxymethyl-2-methoxy-phenoxy)-propoxy]-3,8,13-trimethoxy-10,15-dihydro-5H-tribenzo[a,d,g]cyclononen-2-yloxy}-propoxy)-3-methoxy-phenyl]-methanol (110316-15-9,110352-24-4) → cryptophane-E (102683-14-7,102735-01-3,110352-20-0,155322-30-8) + cryptophane F (102683-15-8)

Guidance literature:

In formic acid; at 60 ℃; for 3h;

DOI:10.1021/ja00274a067

Reference yield: 28.0%

C72H90O18 → cryptophane-E (102683-14-7,102735-01-3,110352-20-0,155322-30-8)

Guidance literature:

With scandium tris(trifluoromethanesulfonate); In dichloromethane; at 60 ℃; for 48h;

DOI:10.1021/jo050495g

upstream raw materials:

[4-(3-{7,12-Bis-[3-(4-hydroxymethyl-2-methoxy-phenoxy)-propoxy]-3,8,13-trimethoxy-10,15-dihydro-5H-tribenzo[a,d,g]cyclononen-2-yloxy}-propoxy)-3-methoxy-phenyl]-methanol

1,3-bis<4-(hydroxymethyl)-2-methoxyphenoxy>propane

cyclotriguaiacyclene

(±)-2,7,12-trimethoxy-3,8,13-tris(2-propenyloxy)-10,15-dihydro-5Htribenzo[a,d,g]cyclononene

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