Silane, (1,1-dimethylethyl)[[2-(1,3-dithian-2-yl)phenyl]thio]dimethyl-

Base Information

Chemical Name:Silane, (1,1-dimethylethyl)[[2-(1,3-dithian-2-yl)phenyl]thio]dimethyl-
CAS No.:765292-75-9
Molecular Formula:C16H26S3Si
Molecular Weight:342.666
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Silane, (1,1-dimethylethyl)[[2-(1,3-dithian-2-yl)phenyl]thio]dimethyl-

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Silane, (1,1-dimethylethyl)[[2-(1,3-dithian-2-yl)phenyl]thio]dimethyl-

There total 7 articles about Silane, (1,1-dimethylethyl)[[2-(1,3-dithian-2-yl)phenyl]thio]dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 765292-73-7
C₂₀H₂₂S₆

: 765292-75-9
2-[2'-(tert-butyldimethylsilylsulfanyl)phenyl]-1.3-dithiane

Guidance literature:: Multi-step reaction with 2 steps

1: 3.69 g / LiAlH₄ / tetrahydrofuran / 1.75 h / 20 °C

2: 65 percent / pyridine / CH₂Cl₂ / 20 °C

With pyridine; lithium aluminium tetrahydride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo049344o

Reference yield:

: 53165-22-3
2-(2'-aminophenyl)-1,3-dithiane

: 765292-75-9
2-[2'-(tert-butyldimethylsilylsulfanyl)phenyl]-1.3-dithiane

Guidance literature:: Multi-step reaction with 2 steps

1.1: HCl; sodium nitrite / H₂O / 0.5 h / 0 - 5 °C

1.2: potassium ethyl xanthate / H₂O / 0.5 h / 40 - 45 °C

1.3: 64 percent / LiAlH₄ / tetrahydrofuran

2.1: 65 percent / pyridine / CH₂Cl₂ / 20 °C

With pyridine; hydrogenchloride; sodium nitrite; In dichloromethane; water;
DOI:10.1021/jo049344o

Reference yield:

: 4521-31-7
o-hydroxymethyl thiophenol

: 765292-75-9
2-[2'-(tert-butyldimethylsilylsulfanyl)phenyl]-1.3-dithiane

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / IBX / ethyl acetate / 2.5 h / 80 °C

2: boron trifluoride etherate; acetic acid / toluene / 4.5 h / 20 °C

3: 3.69 g / LiAlH₄ / tetrahydrofuran / 1.75 h / 20 °C

4: 65 percent / pyridine / CH₂Cl₂ / 20 °C

With pyridine; lithium aluminium tetrahydride; boron trifluoride diethyl etherate; acetic acid; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; dichloromethane; ethyl acetate; toluene;
DOI:10.1021/jo049344o