Benzamide, N-(2-aminophenyl)-4-(hexahydro-4-methyl-1H-1,4-diazepin-1-yl)-

Base Information

Chemical Name:Benzamide, N-(2-aminophenyl)-4-(hexahydro-4-methyl-1H-1,4-diazepin-1-yl)-
CAS No.:766497-44-3
Molecular Formula:C19H24N4O
Molecular Weight:324.42000
Hs Code.:

Synonyms:N-(2-Amino-phenyl)-4-(4-methyl-[1,4]diazepan-1-yl)-benzamide;N-(2-aminophenyl)-4-(1-methylhomopiperazin-4-yl)benzamide;

Suppliers and Price of Benzamide, N-(2-aminophenyl)-4-(hexahydro-4-methyl-1H-1,4-diazepin-1-yl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 2 raw suppliers

Chemical Property of Benzamide, N-(2-aminophenyl)-4-(hexahydro-4-methyl-1H-1,4-diazepin-1-yl)-

Chemical Property:

PSA：61.60000
LogP:3.32010

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of Benzamide, N-(2-aminophenyl)-4-(hexahydro-4-methyl-1H-1,4-diazepin-1-yl)-

There total 2 articles about Benzamide, N-(2-aminophenyl)-4-(hexahydro-4-methyl-1H-1,4-diazepin-1-yl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 730933-25-2
4-(4-methyl-1,4-diazepan-1-yl)benzoic acid

: 95-54-5
1,2-diamino-benzene

: 766497-44-3
N-(2-aminophenyl)-4-(4-methyl-1,4-diazepan-1-yl)benzamide

Guidance literature:: With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In N,N-dimethyl-formamide; at 20 ℃; for 12h;
DOI:10.1016/j.bmc.2004.11.005

Reference yield:

: 166438-80-8
4-(4-Methyl-1,4-diazepan-1-yl)benzonitrile

: 766497-44-3
N-(2-aminophenyl)-4-(4-methyl-1,4-diazepan-1-yl)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / NaOH / 40 h / Heating

2: 89 percent / N-hydroxybenzotriazole; water-soluble carbodiimide / dimethylformamide / 12 h / 20 °C

With sodium hydroxide; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2004.11.005

Reference yield: 70.0%

: 766497-44-3
N-(2-aminophenyl)-4-(4-methyl-1,4-diazepan-1-yl)benzamide

: 24964-64-5
3-Cyanobenzaldehyde

: 840531-09-1
N-{2-[(3-cyanobenzyl)amino]phenyl}-4-(4-methyl-1,4-diazepan-1-yl)benzamide

Guidance literature:: With sodium tris(acetoxy)borohydride; acetic acid; In 1,2-dichloro-ethane; at 20 ℃; for 5h;
DOI:10.1016/j.bmc.2004.11.005