3,4-Dimethoxybenzyl iodide

Base Information

• Chemical Name: 3,4-Dimethoxybenzyl iodide
• CAS No.: 76950-76-0
• Molecular Formula: C9H11IO2
• Molecular Weight: 278.09
• DSSTox Substance ID: DTXSID80457351
• Nikkaji Number: J314.392I
• Wikidata: Q82280176

Synonyms:3,4-dimethoxybenzyl iodide;76950-76-0;SCHEMBL7632612;DTXSID80457351;HMZMWOTUXBSUTC-UHFFFAOYSA-N;1,2-Dimethoxy-4-iodomethylbenzene;AKOS014116339

Chemical Property of 3,4-Dimethoxybenzyl iodide

Chemical Property:

• PSA: 18.46000
• LogP: 2.63880
• XLogP3: 2.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 3
• Exact Mass: 277.98038
• Heavy Atom Count: 12
• Complexity: 130

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: COC1=C(C=C(C=C1)CI)OC

Technology Process of 3,4-Dimethoxybenzyl iodide

There total 6 articles about 3,4-Dimethoxybenzyl iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

(3,4-dimethoxyphenyl)methanol (93-03-8) → 4-(iodomethyl)-1,2-dimethoxybenzene (76950-76-0)

Guidance literature:

With triethylamine sulfate; potassium iodide; for 0.00833333h; Microwave irradiation; Ionic liquid;

DOI:10.1080/00397910802120916

Reference yield: 73.0%

1-(3,4-Dimethoxy-benzyl)-2-methylsulfanyl-4,6-diphenyl-pyridinium; iodide (76950-82-8) → 4-(iodomethyl)-1,2-dimethoxybenzene (76950-76-0)

Guidance literature:

under 1 Torr;

DOI:10.1055/s-1980-29239

Reference yield:

4-chloromethyl-1,2-dimethoxy-benzene (7306-46-9) → 4-(iodomethyl)-1,2-dimethoxybenzene (76950-76-0)

Guidance literature:

With sodium iodide; In acetone; for 12h;

upstream raw materials:

1-(3,4-Dimethoxy-benzyl)-2-methylsulfanyl-4,6-diphenyl-pyridinium; iodide

3,4-dimethoxy-benzaldehyde

4-chloromethyl-1,2-dimethoxy-benzene

(3,4-dimethoxyphenyl)methanol

Downstream raw materials:

(2R,5R)-2-(t-Butyl)-5-(3,4-dimethoxybenzyl)-3-methyl-5-(1-methylethyl)-4-oxo-1-imidazolidincarbonsaeure-t-butylester

(R)-4-(3,4-Dimethoxy-benzyl)-3-((R)-2-methoxy-1-phenyl-ethyl)-oxazolidine-4-carboxylic acid tert-butyl ester

1-(3,4-dimethoxy-benzyl)-cyclopentanecarboxylic acid methyl ester

3-(3,4-dimethoxyphenyl)-1-(5-hydroxy-2,2-dimethyl-2H-chromen-6-yl)propan-1-one

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