2,4-Cyclohexadien-1-one,3-hydroxy-2-(3-hydroxy-1-oxo-3-phenyl-2-propenyl)-5-methoxy-6,6-dimethyl- (9CI)

Base Information

Chemical Name:2,4-Cyclohexadien-1-one,3-hydroxy-2-(3-hydroxy-1-oxo-3-phenyl-2-propenyl)-5-methoxy-6,6-dimethyl- (9CI)
CAS No.:133056-30-1
Molecular Formula:C₁₈H₁₈O₅
Molecular Weight:314.338
Hs Code.:

Synonyms:Syzgiol; Syzygiol

Suppliers and Price of 2,4-Cyclohexadien-1-one,3-hydroxy-2-(3-hydroxy-1-oxo-3-phenyl-2-propenyl)-5-methoxy-6,6-dimethyl- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2,4-Cyclohexadien-1-one,3-hydroxy-2-(3-hydroxy-1-oxo-3-phenyl-2-propenyl)-5-methoxy-6,6-dimethyl- (9CI)

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,4-Cyclohexadien-1-one,3-hydroxy-2-(3-hydroxy-1-oxo-3-phenyl-2-propenyl)-5-methoxy-6,6-dimethyl- (9CI)

There total 5 articles about 2,4-Cyclohexadien-1-one,3-hydroxy-2-(3-hydroxy-1-oxo-3-phenyl-2-propenyl)-5-methoxy-6,6-dimethyl- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.3%

: 144686-11-3
2-(2,3-dibromo-3-phenylpropionyl)-3-hydroxy-5-methoxy-6,6-dimethyl-2,4-cyclohexadien-1-one

: 133056-30-1
syzygiol

Guidance literature:: With sodium hydroxide; In methanol; for 0.166667h; Ambient temperature;
DOI:10.1246/bcsj.65.2552

Reference yield:

: 16302-39-9
2-acetyl-3,5-dihydroxy-4,4-dimethyl-2,5-cyclohexadien-1-one

: 133056-30-1
syzygiol

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / ethyl acetate; diethyl ether / Ambient temperature

2: 79 percent / piperidine / 0.5 h / 85 °C

3: 72.4 percent / Br₂ / CHCl₃ / 0 °C

4: 33.3 percent / 20percent aq. NaOH / methanol / 0.17 h / Ambient temperature

With piperidine; sodium hydroxide; bromine; In methanol; diethyl ether; chloroform; ethyl acetate;
DOI:10.1246/bcsj.65.2552

Reference yield:

: 2999-26-0
2,6-diacetyl-3,5-dihydroxy-4,4-dimethyl-2,5-cyclohexadien-1-one

: 133056-30-1
syzygiol

Guidance literature:: Multi-step reaction with 5 steps

1: 72.6 percent / 80percent H₂SO₄ / Heating

2: 99 percent / ethyl acetate; diethyl ether / Ambient temperature

3: 79 percent / piperidine / 0.5 h / 85 °C

4: 72.4 percent / Br₂ / CHCl₃ / 0 °C

5: 33.3 percent / 20percent aq. NaOH / methanol / 0.17 h / Ambient temperature

With piperidine; sodium hydroxide; sulfuric acid; bromine; In methanol; diethyl ether; chloroform; ethyl acetate;
DOI:10.1246/bcsj.65.2552