1-Piperazinecarboxylic acid, 4-[4-[3-[(2-methoxyphenyl)methoxy]propoxy]phenyl]-3-oxo-5-[[[(trifluoro methyl)sulfonyl]oxy]methyl]-, 1,1-dimethylethyl ester, (5R)-

Base Information

Chemical Name:1-Piperazinecarboxylic acid, 4-[4-[3-[(2-methoxyphenyl)methoxy]propoxy]phenyl]-3-oxo-5-[[[(trifluoro methyl)sulfonyl]oxy]methyl]-, 1,1-dimethylethyl ester, (5R)-
CAS No.:777934-65-3
Molecular Formula:C28H35F3N2O9S
Molecular Weight:632.655
Hs Code.:

1-Piperazinecarboxylic acid,
4-[4-[3-[(2-methoxyphenyl)methoxy]propoxy]phenyl]-3-oxo-5-[[[(trifluoro
methyl)sulfonyl]oxy]methyl]-, 1,1-dimethylethyl ester, (5R)-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Piperazinecarboxylic acid, 4-[4-[3-[(2-methoxyphenyl)methoxy]propoxy]phenyl]-3-oxo-5-[[[(trifluoro methyl)sulfonyl]oxy]methyl]-, 1,1-dimethylethyl ester, (5R)-

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Technology Process of 1-Piperazinecarboxylic acid, 4-[4-[3-[(2-methoxyphenyl)methoxy]propoxy]phenyl]-3-oxo-5-[[[(trifluoro methyl)sulfonyl]oxy]methyl]-, 1,1-dimethylethyl ester, (5R)-

There total 1 articles about 1-Piperazinecarboxylic acid, 4-[4-[3-[(2-methoxyphenyl)methoxy]propoxy]phenyl]-3-oxo-5-[[[(trifluoro methyl)sulfonyl]oxy]methyl]-, 1,1-dimethylethyl ester, (5R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.44%

: 777934-38-0
(3R)-3-hydroxymethyl-4-{4-[3-(2-methoxybenzyloxy)-propoxy]-phenyl}-5-oxopiperazine-1-carboxylic acid tert-butyl ester

: 358-23-6
trifluoromethylsulfonic anhydride

: 777934-65-3
(5R)-4-(4-[3-(2-methoxybenzyloxy)propoxy]phenyl)-3-oxo-5-trifluoromethanesulfonyloxypiperazine-1-carboxylic acid tert-butyl ester

Guidance literature:: (3R)-3-hydroxymethyl-4-{4-[3-(2-methoxybenzyloxy)-propoxy]-phenyl}-5-oxopiperazine-1-carboxylic acid tert-butyl ester; In dichloromethane; at -78 ℃; Cooling with acetone-dry ice;

trifluoromethylsulfonic anhydride; In dichloromethane; at 20 ℃; for 0.25h;