2-Propanone, 1-(2-acetyl-3,6-dimethoxyphenyl)-

Base Information

Chemical Name:2-Propanone, 1-(2-acetyl-3,6-dimethoxyphenyl)-
CAS No.:78572-88-0
Molecular Formula:C13H16O4
Molecular Weight:236.268
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Propanone, 1-(2-acetyl-3,6-dimethoxyphenyl)-

Chemical Property:

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Technology Process of 2-Propanone, 1-(2-acetyl-3,6-dimethoxyphenyl)-

There total 3 articles about 2-Propanone, 1-(2-acetyl-3,6-dimethoxyphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 78572-87-9
4,7-dimethoxy-2,3-dimethylindene

: 78572-88-0
3-acetonyl-2-acetyl-1,4-dimethoxybenzene

Guidance literature:: With sodium periodate; osmium(VIII) oxide; Yield given. Multistep reaction; 1.) dioxan, water, room temperature, 5 min, 2.) 3 days;
DOI:10.1039/P19810001191

Reference yield:

: 78572-86-8
4,7-dihydroxy-2-methyl-indan-1-one

: 78572-88-0
3-acetonyl-2-acetyl-1,4-dimethoxybenzene

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / 2M-sodium hydroxide / 1.) room temperature, 30 min, 2.) 70 deg C, 10 min

2: 2.) 10percent hydrochloric acid / 1.) ether, room temperature, 50 min, 2.) 2 min

3: 1.) osmium tetraoxide, 2.) sodium metaperiodate / 1.) dioxan, water, room temperature, 5 min, 2.) 3 days

With hydrogenchloride; sodium hydroxide; sodium periodate; osmium(VIII) oxide;
DOI:10.1039/P19810001191

Reference yield:

: 59743-69-0
4,7-dimethoxy-2-methylindan-1-one

: 78572-88-0
3-acetonyl-2-acetyl-1,4-dimethoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 2.) 10percent hydrochloric acid / 1.) ether, room temperature, 50 min, 2.) 2 min

2: 1.) osmium tetraoxide, 2.) sodium metaperiodate / 1.) dioxan, water, room temperature, 5 min, 2.) 3 days

With hydrogenchloride; sodium periodate; osmium(VIII) oxide;
DOI:10.1039/P19810001191