Benzenesulfonic acid, 2,4,6-trimethyl-, silver(1+) salt

Base Information

Chemical Name:Benzenesulfonic acid, 2,4,6-trimethyl-, silver(1+) salt
CAS No.:78907-59-2
Molecular Formula:C9H12O3S.Ag
Molecular Weight:307.119
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenesulfonic acid, 2,4,6-trimethyl-, silver(1+) salt

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of Benzenesulfonic acid, 2,4,6-trimethyl-, silver(1+) salt

There total 1 articles about Benzenesulfonic acid, 2,4,6-trimethyl-, silver(1+) salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3453-83-6
mesitylene sulfonic acid

: silver nitrate

: 78907-59-2
solver 2,4,6-trimethylbenzenesulfonate

Guidance literature:: With Na₂CO₃; In water; (N2); addn. of sodium carbonate to aq. soln. of sulfonic acid deriv., stirring, addn. of silver compd.; filtration, washing with cold water, drying in vac. at 60°C overnight;
DOI:10.1021/om1007924

Reference yield: 94.0%

: 80520-49-6
iodo-1 pentanone-2

: 78907-59-2
solver 2,4,6-trimethylbenzenesulfonate

: 80519-93-3
1-(2,4,6-trimethylbenzenesulfonyloxy)-2-pentanone

Guidance literature:: In acetonitrile; for 40h; Ambient temperature;
DOI:10.1248/cpb.34.1118

Reference yield: 82.0%

: Stewart-Grubbs catalyst

: 78907-59-2
solver 2,4,6-trimethylbenzenesulfonate

: [RuCl(mesitylsulfonate)(CHC₆H₄OiPr)(C₃H₄N₂(C₆H₄Me))]

Guidance literature:: In benzene; byproducts: AgCl; (N2); addn. of silver compd. to benzene soln. of ruthenium compd., stirring for 5 h; filtration through celite, evapn. in vac., NMR and MS;
DOI:10.1021/om1007924