Methanone, [1-bromo-2-(3-chloro-4-methylphenyl)-3-indolizinyl][3,5-dibromo-4-[3-(di butylamino)propoxy]phenyl]-, ethanedioate (1:1)

Base Information

Chemical Name:Methanone, [1-bromo-2-(3-chloro-4-methylphenyl)-3-indolizinyl][3,5-dibromo-4-[3-(di butylamino)propoxy]phenyl]-, ethanedioate (1:1)
CAS No.:79283-45-7
Molecular Formula:C33H36Br3ClN2O2.C2H2O4
Molecular Weight:857.862
Hs Code.:

Synonyms:

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Chemical Property of Methanone, [1-bromo-2-(3-chloro-4-methylphenyl)-3-indolizinyl][3,5-dibromo-4-[3-(di butylamino)propoxy]phenyl]-, ethanedioate (1:1)

Chemical Property:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of Methanone, [1-bromo-2-(3-chloro-4-methylphenyl)-3-indolizinyl][3,5-dibromo-4-[3-(di butylamino)propoxy]phenyl]-, ethanedioate (1:1)

There total 3 articles about Methanone, [1-bromo-2-(3-chloro-4-methylphenyl)-3-indolizinyl][3,5-dibromo-4-[3-(di butylamino)propoxy]phenyl]-, ethanedioate (1:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.4%

: 36421-15-5
dibutyl-(3-chloro-propyl)-amine

: 77833-20-6
[1-Bromo-2-(3-chloro-4-methyl-phenyl)-indolizin-3-yl]-(3,5-dibromo-4-hydroxy-phenyl)-methanone

: 79283-45-7
[1-Bromo-2-(3-chloro-4-methyl-phenyl)-indolizin-3-yl]-[3,5-dibromo-4-(3-dibutylamino-propoxy)-phenyl]-methanone; compound with oxalic acid

Guidance literature:: With potassium carbonate; In acetone; for 20h; Heating;

Reference yield:

: 64676-51-3
[2-(3-Chloro-4-methyl-phenyl)-indolizin-3-yl]-(4-hydroxy-phenyl)-methanone

: 79283-45-7
[1-Bromo-2-(3-chloro-4-methyl-phenyl)-indolizin-3-yl]-[3,5-dibromo-4-(3-dibutylamino-propoxy)-phenyl]-methanone; compound with oxalic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 19.3 percent / Br₂, sodium acetate trihydrate / acetic acid / 2 h / 20 - 30 °C

2: 19.2 percent / Br₂, sodium acetate / dioxane / 1 h / 20 - 22 °C

3: 81.4 percent / potassium carbonate / acetone / 20 h / Heating

With bromine; sodium acetate; potassium carbonate; In 1,4-dioxane; acetic acid; acetone;

Reference yield:

: 77832-63-4
[1-Bromo-2-(3-chloro-4-methyl-phenyl)-indolizin-3-yl]-(4-hydroxy-phenyl)-methanone

: 79283-45-7
[1-Bromo-2-(3-chloro-4-methyl-phenyl)-indolizin-3-yl]-[3,5-dibromo-4-(3-dibutylamino-propoxy)-phenyl]-methanone; compound with oxalic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 19.2 percent / Br₂, sodium acetate / dioxane / 1 h / 20 - 22 °C

2: 81.4 percent / potassium carbonate / acetone / 20 h / Heating

With bromine; sodium acetate; potassium carbonate; In 1,4-dioxane; acetone;