3'-Thymidylic acid, 5'-O-(triphenylmethyl)-, 2-(2-chloro-4-nitrophenyl)ethyl 4-nitrophenyl ester

Base Information

Chemical Name:3'-Thymidylic acid, 5'-O-(triphenylmethyl)-, 2-(2-chloro-4-nitrophenyl)ethyl 4-nitrophenyl ester
CAS No.:79536-90-6
Molecular Formula:C₄₃H₃₈ClN₄O₁₂P
Molecular Weight:869.221
Hs Code.:

Synonyms:

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Chemical Property of 3'-Thymidylic acid, 5'-O-(triphenylmethyl)-, 2-(2-chloro-4-nitrophenyl)ethyl 4-nitrophenyl ester

Chemical Property:

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Technology Process of 3'-Thymidylic acid, 5'-O-(triphenylmethyl)-, 2-(2-chloro-4-nitrophenyl)ethyl 4-nitrophenyl ester

There total 6 articles about 3'-Thymidylic acid, 5'-O-(triphenylmethyl)-, 2-(2-chloro-4-nitrophenyl)ethyl 4-nitrophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 777-52-6
1-dichlorophosphoryloxy-4-nitro-benzene

: 79536-90-6
(5'-O-Trityl-thymidin-3')(2-chlor-4-nitrophenylaethyl)(p-nitrophenyl)phosphorsaeureester

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 2 h / Ambient temperature

2: pyridine / 1.5 h / Ambient temperature

3: pyridine / 20 h / Ambient temperature

With pyridine; In pyridine;
DOI:10.1002/hlca.19810640547

Reference yield:

: 104-30-3
2-(4-nitrophenyl)ethyl acetate

: 79536-90-6
(5'-O-Trityl-thymidin-3')(2-chlor-4-nitrophenylaethyl)(p-nitrophenyl)phosphorsaeureester

Guidance literature:: Multi-step reaction with 3 steps

1: Cl₂, CH₃COONa / trifluoroacetic acid; CCl₄ / 3 h / Ambient temperature

2: HCl / methanol / 1 h / Heating

3: pyridine / 20 h / Ambient temperature

With hydrogenchloride; sodium acetate; chlorine; In pyridine; methanol; tetrachloromethane; trifluoroacetic acid;
DOI:10.1002/hlca.19810640547

Reference yield:

: 103-45-7
acetic acid phenethyl ester

: 79536-90-6
(5'-O-Trityl-thymidin-3')(2-chlor-4-nitrophenylaethyl)(p-nitrophenyl)phosphorsaeureester

Guidance literature:: Multi-step reaction with 4 steps

1: H₂SO₄, HNO₃ / acetic anhydride / 1.75 h / -15 °C

2: Cl₂, CH₃COONa / trifluoroacetic acid; CCl₄ / 3 h / Ambient temperature

3: HCl / methanol / 1 h / Heating

4: pyridine / 20 h / Ambient temperature

With hydrogenchloride; sulfuric acid; nitric acid; sodium acetate; chlorine; In pyridine; methanol; tetrachloromethane; acetic anhydride; trifluoroacetic acid;
DOI:10.1002/hlca.19810640547