Prop-2-en-1-yl triphenylstannanecarbodithioate

Base Information

Chemical Name:Prop-2-en-1-yl triphenylstannanecarbodithioate
CAS No.:79634-85-8
Molecular Formula:C₂₂H₂₀S₂Sn
Molecular Weight:467.243
Hs Code.:
DSSTox Substance ID:DTXSID80541885
Wikidata:Q82418350

Synonyms:79634-85-8;Prop-2-en-1-yl triphenylstannanecarbodithioate;DTXSID80541885

Suppliers and Price of Prop-2-en-1-yl triphenylstannanecarbodithioate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Prop-2-en-1-yl triphenylstannanecarbodithioate

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:7
Exact Mass:468.002846
Heavy Atom Count:25
Complexity:384

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C=CCSC(=S)[Sn](C1=CC=CC=C1)(C2=CC=CC=C2)C3=CC=CC=C3

Technology Process of Prop-2-en-1-yl triphenylstannanecarbodithioate

There total 3 articles about Prop-2-en-1-yl triphenylstannanecarbodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 75-15-0,12122-00-8
carbon disulfide

: 4167-90-2
lithium triphenylstannide

: 106-95-6
allyl bromide

: 79634-85-8
allyl triphenylstannanedithiocarboxylate

Guidance literature:: In tetrahydrofuran; byproducts: LiBr; to (C6H5)3SnLi in THF dropped under stirring CS2 in slight excess, colour change to red brown with warmingp, after cooling addn. of C3H5Br in excess; column chromy. (silica gel/THF), solvent removed from the violet fraction, treated with ethanol, pptn., recrystd. from petroleum ether, elem. anal.;

Reference yield:

: 76-63-1
allytriphenyltin

: 79634-85-8
allyl triphenylstannanedithiocarboxylate

Guidance literature:: With carbon disulfide; In not given; elem. anal.;

Reference yield:

: 84448-52-2
(C₆H₅)3SnCS₂^(1-)*Li⁽¹⁺⁾=(C₆H₅)3SnCS₂Li

: 106-95-6
allyl bromide

: 79634-85-8
allyl triphenylstannanedithiocarboxylate

Guidance literature:: In tetrahydrofuran; under N2, C3H5Br added to soln. of Sn-compd. in THF; modified from Kunze, U.; Bolz, P.-R.; Winter, W. Chem. Ber. 1981, 114, 2744; evapd. to dryness, extd. with petroleum ether, vol. reduced by evapn., washed with hexane;