4-Bromo-2-{[(4-ethoxyphenyl)imino]methyl}phenol

Base Information

• Chemical Name: 4-Bromo-2-{[(4-ethoxyphenyl)imino]methyl}phenol
• CAS No.: 4718-19-8
• Molecular Formula: C₁₅H₁₄BrNO₂
• Molecular Weight: 320.186
• NSC Number: 201829
• DSSTox Substance ID: DTXSID00419850
• Wikidata: Q82231065

Synonyms:4718-19-8;NSC201829;4-bromo-2-{[(4-ethoxyphenyl)imino]methyl}phenol;4-bromo-6-{[(4-ethoxyphenyl)amino]methylene}-2,4-cyclohexadien-1-one;SCHEMBL12416695;DTXSID00419850;AKOS002286523;NSC-201829;4-BROMO-2-((4-ETHOXY-PHENYLIMINO)-METHYL)-PHENOL

Chemical Property of 4-Bromo-2-{[(4-ethoxyphenyl)imino]methyl}phenol

Chemical Property:

• Vapor Pressure: 1.87E-06mmHg at 25°C
• Boiling Point: 395.2°Cat760mmHg
• Flash Point: 192.8°C
• Density: 1.547g/cm³
• XLogP3: 3.9
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 4
• Exact Mass: 319.02079
• Heavy Atom Count: 19
• Complexity: 290

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCOC1=CC=C(C=C1)N=CC2=C(C=CC(=C2)Br)O

Technology Process of 4-Bromo-2-{[(4-ethoxyphenyl)imino]methyl}phenol

There total 3 articles about 4-Bromo-2-{[(4-ethoxyphenyl)imino]methyl}phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

salicylaldehyde (90-02-8) → 2-[(4-ethoxy-phenylimino)-methyl]-4-bromo-phenol (4718-19-8)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrachloromethane; bromine

2: ethanol

With tetrachloromethane; ethanol; bromine;

DOI:10.1021/ja01329a049

Reference yield:

4-Ethoxyaniline (156-43-4) + 5-bromosalicyclaldehyde (1761-61-1) → 2-[(4-ethoxy-phenylimino)-methyl]-4-bromo-phenol (4718-19-8)

Guidance literature:

With ethanol;

DOI:10.1021/ja01329a049

Reference yield:

→ 2-[(4-ethoxy-phenylimino)-methyl]-4-bromo-phenol (4718-19-8)

Guidance literature:

Malonsaeure-mono-p-phenetidid, 5-Brom-salicylaldehyd, wenig Py., neben 6-Brom-cumarin-3-carbonsaeure-p-phenetidid;

upstream raw materials:

4-Ethoxyaniline

5-bromosalicyclaldehyde

salicylaldehyde

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