Benzene, 1-(3-chloro-3-methyl-1-butynyl)-4-methyl-

Base Information

Chemical Name:Benzene, 1-(3-chloro-3-methyl-1-butynyl)-4-methyl-
CAS No.:79756-93-7
Molecular Formula:C12H13Cl
Molecular Weight:192.688
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzene, 1-(3-chloro-3-methyl-1-butynyl)-4-methyl-

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Technology Process of Benzene, 1-(3-chloro-3-methyl-1-butynyl)-4-methyl-

There total 3 articles about Benzene, 1-(3-chloro-3-methyl-1-butynyl)-4-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 79756-91-5
2-methyl-4-(4-methylphenyl)-3-butyn-2-ol

: 79756-93-7
1-(3-Chloro-3-methyl-but-1-ynyl)-4-methyl-benzene

Guidance literature:: With hydrogenchloride; copper; copper(l) chloride; calcium chloride; In diethyl ether; Petroleum ether; at 5 ℃; for 1h;

Reference yield:

: 65114-80-9
1-(4-Methylphenyl)-1,1-dichlorethan

: 79756-93-7
1-(3-Chloro-3-methyl-but-1-ynyl)-4-methyl-benzene

Guidance literature:: Multi-step reaction with 3 steps

1: 53 percent / KOH / ethanol / Heating

2: 1.) MeI, Li / 1.) Et₂O, 20 deg C, 1 h; 2.) 20 deg C, 12 h

3: 84 percent / CaCl₂, CuCl, Cu, 12N HCl / diethyl ether; petroleum ether / 1 h / 5 °C

With hydrogenchloride; potassium hydroxide; lithium; copper; copper(l) chloride; calcium chloride; methyl iodide; In diethyl ether; ethanol; Petroleum ether;

Reference yield:

: 122-00-9
para-methylacetophenone

: 79756-93-7
1-(3-Chloro-3-methyl-but-1-ynyl)-4-methyl-benzene

Guidance literature:: Multi-step reaction with 4 steps

1: 76 percent / PCl₅ / 12 h / 20 °C

2: 53 percent / KOH / ethanol / Heating

3: 1.) MeI, Li / 1.) Et₂O, 20 deg C, 1 h; 2.) 20 deg C, 12 h

4: 84 percent / CaCl₂, CuCl, Cu, 12N HCl / diethyl ether; petroleum ether / 1 h / 5 °C

With hydrogenchloride; potassium hydroxide; phosphorus pentachloride; lithium; copper; copper(l) chloride; calcium chloride; methyl iodide; In diethyl ether; ethanol; Petroleum ether;