1H-Pyrrole, 1-(4-azido-2-fluorophenyl)-

Base Information

Chemical Name:1H-Pyrrole, 1-(4-azido-2-fluorophenyl)-
CAS No.:797783-49-4
Molecular Formula:C10H7FN4
Molecular Weight:202.191
Hs Code.:

Synonyms:

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Chemical Property of 1H-Pyrrole, 1-(4-azido-2-fluorophenyl)-

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Technology Process of 1H-Pyrrole, 1-(4-azido-2-fluorophenyl)-

There total 6 articles about 1H-Pyrrole, 1-(4-azido-2-fluorophenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 797783-48-3
4-azido-2-fluoro-phenylamine

: 2,4-dimethoxytetrahydrofuran

: 797783-49-4
1-(4-azido-2-fluorophenyl)-1H-pyrrole

Guidance literature:: With acetic acid; at 114 ℃; for 4h; Heating;

Reference yield:

: C₁₄H₇FN₃O₂⁽¹⁺⁾*Cl^(1-)

: 797783-49-4
1-(4-azido-2-fluorophenyl)-1H-pyrrole

Guidance literature:: Multi-step reaction with 3 steps

1: sodium azide; sodium acetate / water

2: hydrazine / methanol / 2 h / Heating / reflux

3: acetic acid / 4 h / 114 °C / Heating

With sodium azide; sodium acetate; acetic acid; hydrazine; In methanol; water;

Reference yield:

: 369-34-6
3,4-difluoronitrobenzene

: 797783-49-4
1-(4-azido-2-fluorophenyl)-1H-pyrrole

Guidance literature:: Multi-step reaction with 6 steps

1: DMF (N,N-dimethyl-formamide) / 4 h / 100 °C / Heating

2: palladium 10% on activated carbon; ammonium formate / tetrahydrofuran; methanol / 1 h / 0 - 20 °C

3: hydrogenchloride; sodium nitrite / water / 1 h / 0 °C

4: sodium azide; sodium acetate / water

5: hydrazine / methanol / 2 h / Heating / reflux

6: acetic acid / 4 h / 114 °C / Heating

With hydrogenchloride; sodium azide; palladium 10% on activated carbon; ammonium formate; sodium acetate; acetic acid; hydrazine; sodium nitrite; In tetrahydrofuran; methanol; DMF (N,N-dimethyl-formamide); water;