3-[[p-(diethylamino)phenyl]azo]-1,4-dimethyl-1H-1,2,4-triazolium chloride

Base Information

Chemical Name:3-[[p-(diethylamino)phenyl]azo]-1,4-dimethyl-1H-1,2,4-triazolium chloride
CAS No.:29120-27-2
Molecular Formula:C14H21 N6 . Cl
Molecular Weight:308.814
Hs Code.:
Mol file:29120-27-2.mol

Synonyms:1H-1,2,4-Triazolium,3-[[4-(diethylamino)phenyl]azo]-1,4-dimethyl-, chloride (9CI);1H-1,2,4-Triazolium, 3-[[p-(diethylamino)phenyl]azo]-1,4-dimethyl-, chloride(8CI); 3-(p-Diethylaminophenylazo)-1,4-dimethyl-1,2,4-triazolinium chloride

Suppliers and Price of 3-[[p-(diethylamino)phenyl]azo]-1,4-dimethyl-1H-1,2,4-triazolium chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 5 raw suppliers

Chemical Property of 3-[[p-(diethylamino)phenyl]azo]-1,4-dimethyl-1H-1,2,4-triazolium chloride

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
PSA：49.66000
Density:g/cm³
LogP:-0.48980

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-[[p-(diethylamino)phenyl]azo]-1,4-dimethyl-1H-1,2,4-triazolium chloride

There total 3 articles about 3-[[p-(diethylamino)phenyl]azo]-1,4-dimethyl-1H-1,2,4-triazolium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 77-78-1
dimethyl sulfate

: Diethyl-[4-(4-methyl-4H-[1,2,4]triazol-3-ylazo)-phenyl]-amine

: 29120-27-2
cationic red S

: basic red 22

Guidance literature:: With magnesium oxide; sodium chloride; zinc(II) chloride; In acetic acid; at 80 - 90 ℃; for 1h;

Reference yield:

: 77-78-1
dimethyl sulfate

: Diethyl-[4-(4H-[1,2,4]triazol-3-ylazo)-phenyl]-amine

: 29120-27-2
cationic red S

: basic red 22

Guidance literature:: With magnesium oxide; In acetic acid; at 80 - 90 ℃; Yield given. Yields of byproduct given;

Reference yield:

: 91-66-7
N,N-diethylaniline

: 29120-27-2
cationic red S

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) conc. H₂SO₄, 5N NaNO₂, 2.) 10percent HCl / 1.) H₂₀, glacial acetic acid, 0 deg C - 5 deg C, 2.) H₂O, glacial acetic acid, below 5 deg C

2: MgO / acetic acid / 80 - 90 °C

With hydrogenchloride; sulfuric acid; magnesium oxide; sodium nitrite; In acetic acid;