Azonino[5,4-b]indol-4(1H)-one, 3-benzoyl-2,3,5,6,7,8-hexahydro-8-(tetrahydro-2H-pyran-2-yl)-

Base Information Edit

Chemical Name:Azonino[5,4-b]indol-4(1H)-one, 3-benzoyl-2,3,5,6,7,8-hexahydro-8-(tetrahydro-2H-pyran-2-yl)-
CAS No.:80053-46-9
Molecular Formula:C26H28N2O3
Molecular Weight:416.52
Hs Code.:
Mol file:80053-46-9.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Azonino[5,4-b]indol-4(1H)-one, 3-benzoyl-2,3,5,6,7,8-hexahydro-8-(tetrahydro-2H-pyran-2-yl)- Edit

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of Azonino[5,4-b]indol-4(1H)-one, 3-benzoyl-2,3,5,6,7,8-hexahydro-8-(tetrahydro-2H-pyran-2-yl)-

There total 11 articles about Azonino[5,4-b]indol-4(1H)-one, 3-benzoyl-2,3,5,6,7,8-hexahydro-8-(tetrahydro-2H-pyran-2-yl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 110-87-2
3,4-dihydro-2H-pyran

: 80053-48-1
3-benzoyl-4-oxo-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indole

: 80053-46-9
3-benzoyl-4-oxo-8-(2-tetrahydropyranyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indole

Guidance literature:: With camphor-10-sulfonic acid; In dichloromethane; for 8h; Ambient temperature;
DOI:10.1016/S0040-4020(01)88604-X

Reference yield:

: 73608-98-7
6,7,9,10,11,12-Hexahydro-5H-7,12-diaza-cyclonona[a]inden-8-one

: 80053-46-9
3-benzoyl-4-oxo-8-(2-tetrahydropyranyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indole

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / Et₃N / tetrahydrofuran / Ambient temperature

2: 89 percent / camforsulfonic acid / CH₂Cl₂ / 8 h / Ambient temperature

With camphor-10-sulfonic acid; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja00413a049

Reference yield:

: 89650-66-8
6-oxo-6,7,8,9-tetrahydro-pyrido(1,2-a)indole-10-propionic-acid

: 80053-46-9
3-benzoyl-4-oxo-8-(2-tetrahydropyranyl)-1,2,3,4,5,6,7,8-octahydroazonino<5,4-b>indole

Guidance literature:: Multi-step reaction with 4 steps

2: 80 percent / methanol / 18 h / Irradiation

3: 77 percent / Et₃N / tetrahydrofuran / Ambient temperature

4: 89 percent / camforsulfonic acid / CH₂Cl₂ / 8 h / Ambient temperature

With camphor-10-sulfonic acid; triethylamine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/ja00413a049