(3-chlorophenyl)(2-hydroxy-5-methylphenyl)methanone

Base Information

• Chemical Name: (3-chlorophenyl)(2-hydroxy-5-methylphenyl)methanone
• CAS No.: 6280-54-2
• Molecular Formula: C14H11 Cl O2
• Molecular Weight: 246.693

Synonyms:Benzophenone, 3'-chloro-2-hydroxy-5-methyl- (6CI,8CI);3'-Chloro-2-hydroxy-5-methylbenzophenone; NSC 11163

Chemical Property of (3-chlorophenyl)(2-hydroxy-5-methylphenyl)methanone

Chemical Property:

• Vapor Pressure: 2.27E-06mmHg at 25°C
• Boiling Point: 381.7°C at 760 mmHg
• Flash Point: 184.6°C
• Density: 1.27g/cm³

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (3-chlorophenyl)(2-hydroxy-5-methylphenyl)methanone

There total 3 articles about (3-chlorophenyl)(2-hydroxy-5-methylphenyl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

3-chloro-2-methyl-benzoic acid phenyl ester → 3'-chloro-2-hydroxy-5-methyl-benzophenone (6280-54-2)

Guidance literature:

With Montmorrilonite k 10 clay; microwave irradiation;

DOI:10.1016/j.bmcl.2005.06.012

Reference yield: 90.0%

4-methylphenyl 3-chlorobenzoate (6280-49-5) → 3'-chloro-2-hydroxy-5-methyl-benzophenone (6280-54-2)

Guidance literature:

With aluminium trichloride; In nitrobenzene; at 80 - 90 ℃; for 0.75h;

DOI:10.1016/j.bmc.2007.02.051

Reference yield:

→ 3'-chloro-2-hydroxy-5-methyl-benzophenone (6280-54-2)

Guidance literature:

3-Chlor-benzoesaeure-p-tolylester, AlCl3 (120 u. 160grad);

upstream raw materials:

4-methylphenyl 3-chlorobenzoate

Downstream raw materials:

2-(3-chloro-benzyl)-4-methyl-phenol

ethyl [2-(3-chlorobenzoyl)-4-methylphenoxy]acetate

3-chloro-benzoic acid 2-(3-chloro-benzoyl)-4-methyl-phenyl ester

[2-(3-chlorobenzoyl)-4-methylphenoxy]ethanoic acid

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