3-Methoxy-2-(2-methoxybenzoyl)benzoic acid

Base Information

Chemical Name:3-Methoxy-2-(2-methoxybenzoyl)benzoic acid
CAS No.:80764-46-1
Molecular Formula:C16H14O5
Molecular Weight:286.284
Hs Code.:
DSSTox Substance ID:DTXSID50513256
Wikidata:Q82372964

Synonyms:3-Methoxy-2-(2-methoxybenzoyl)benzoic acid;80764-46-1;DTXSID50513256

Suppliers and Price of 3-Methoxy-2-(2-methoxybenzoyl)benzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 3-Methoxy-2-(2-methoxybenzoyl)benzoic acid

Chemical Property:

XLogP3:2.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:5
Exact Mass:286.08412354
Heavy Atom Count:21
Complexity:381

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=CC=C1C(=O)C2=C(C=CC=C2OC)C(=O)O

Technology Process of 3-Methoxy-2-(2-methoxybenzoyl)benzoic acid

There total 4 articles about 3-Methoxy-2-(2-methoxybenzoyl)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 1206192-62-2
N,N-(diethyl)-2-(2-methoxybenzoyl)-3-methoxybenzene-1-carboxamide

: 80764-46-1
2-(2-methoxybenzoyl)-3-methoxybenzoic acid

Guidance literature:: With hydrogenchloride; In water; for 45h; Inert atmosphere; Reflux;
DOI:10.1002/ejoc.200900960

Reference yield:

: [2-(4,4-Dimethyl-4,5-dihydro-oxazol-2-yl)-6-methoxy-phenyl]-(2-methoxy-phenyl)-methanone

: 80764-46-1
2-(2-methoxybenzoyl)-3-methoxybenzoic acid

Guidance literature:: With hydrogenchloride; Yield given; Heating; overnight;
DOI:10.1021/jo00347a046

Reference yield:

: 73453-77-7
3-(4,4-dimethyloxazolin 2-yl)anisole

: 80764-46-1
2-(2-methoxybenzoyl)-3-methoxybenzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) BuLi / 1.) THF, -45 deg C, 2.) -100 deg C

2: 5percent aq. HCl / Heating; overnight

With hydrogenchloride; n-butyllithium;
DOI:10.1021/jo00347a046