Nitrous acid, (4-nitrophenyl)methyl ester

Base Information

• Chemical Name: Nitrous acid, (4-nitrophenyl)methyl ester
• CAS No.: 80826-97-7
• Molecular Formula: C7H6N2O4
• Molecular Weight: 182.136
• Mol file: 80826-97-7.mol

Synonyms:

Chemical Property of Nitrous acid, (4-nitrophenyl)methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Nitrous acid, (4-nitrophenyl)methyl ester

There total 1 articles about Nitrous acid, (4-nitrophenyl)methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

4-nitrobenzyl chloride (619-73-8) → p-nitrobenzyl nitrite (80826-97-7)

Guidance literature:

With triphenylphosphine; tetrabutylammonium nitrite; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In acetonitrile; for 24h; Heating;

DOI:10.1055/s-2004-829122

Reference yield:

p-nitrobenzyl nitrite (80826-97-7) → 4-nitrobenzyl chloride (619-73-8)

Guidance literature:

With tert-butyl alcohol; In chloroform; at 26 ℃; Equilibrium constant;

DOI:10.1021/jo00168a002

Reference yield:

p-nitrobenzyl nitrite (80826-97-7) → 4-nitrobenzaldehdye (555-16-8)

Guidance literature:

bei 4-taegigem Aufbewahren erfolgt Zersetzung;

DOI:10.1021/jo01102a605

upstream raw materials:

4-nitrobenzyl chloride

Downstream raw materials:

4-nitrobenzyl chloride

4-nitrobenzaldehdye

Refernces

• 1、 Doyle, Michael P.,Terpstra, Jan W.,Pickering, Ruth A.,LePoire, Diane M.. "Hydrolysis, Nitrosyl Exchange, and Synthesis of Alkyl Nitrites". . p. 3379 - 3382. Retrieved 2007/10/02.